Technology Process of 3-(2,5,6-trimethoxy-1-phenyl-1H-inden-3-yl)oxazolidin-2-one
There total 7 articles about 3-(2,5,6-trimethoxy-1-phenyl-1H-inden-3-yl)oxazolidin-2-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris(p-trifluoromethylphenyl)phosphine gold bis(trifluoromethanesulfonyl)imidate;
In
dichloromethane;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1002/chem.201403040
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / Cooling with ice
1.2: 2 h / 20 °C
2.1: potassium carbonate; methanol / 1 h / 20 °C
3.1: N-Bromosuccinimide; silver nitrate / acetone / 1 h / 20 °C
4.1: potassium carbonate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate / toluene / 65 °C
5.1: tris(p-trifluoromethylphenyl)phosphine gold bis(trifluoromethanesulfonyl)imidate / dichloromethane / 1 h / 20 °C / Inert atmosphere
With
methanol; N-Bromosuccinimide; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; tris(p-trifluoromethylphenyl)phosphine gold bis(trifluoromethanesulfonyl)imidate; sodium hydride; potassium carbonate; silver nitrate;
In
tetrahydrofuran; dichloromethane; acetone; toluene; mineral oil;
DOI:10.1002/chem.201403040
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate / toluene / 65 °C
2: tris(p-trifluoromethylphenyl)phosphine gold bis(trifluoromethanesulfonyl)imidate / dichloromethane / 1 h / 20 °C / Inert atmosphere
With
1,10-Phenanthroline; copper(ll) sulfate pentahydrate; tris(p-trifluoromethylphenyl)phosphine gold bis(trifluoromethanesulfonyl)imidate; potassium carbonate;
In
dichloromethane; toluene;
DOI:10.1002/chem.201403040
