(αS)-α-[1,1-dimethyl-2-[(S)-(4-methylphenyl)sulfinyl]-2-propenyl]-2-furanmethanol

Base Information

Chemical Name:(αS)-α-[1,1-dimethyl-2-[(S)-(4-methylphenyl)sulfinyl]-2-propenyl]-2-furanmethanol
CAS No.:887307-88-2
Molecular Formula:C₁₇H₂₀O₃S
Molecular Weight:304.41
Hs Code.:

Synonyms:(αS)-α-[1,1-dimethyl-2-[(S)-(4-methylphenyl)sulfinyl]-2-propenyl]-2-furanmethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (αS)-α-[1,1-dimethyl-2-[(S)-(4-methylphenyl)sulfinyl]-2-propenyl]-2-furanmethanol

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Technology Process of (αS)-α-[1,1-dimethyl-2-[(S)-(4-methylphenyl)sulfinyl]-2-propenyl]-2-furanmethanol

There total 2 articles about (αS)-α-[1,1-dimethyl-2-[(S)-(4-methylphenyl)sulfinyl]-2-propenyl]-2-furanmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 98-01-1
furfural

: 75-11-6
diiodomethane

: 75-16-1
methylmagnesium bromide

: 157070-41-2
1-Methyl-4-((S)-prop-1-yne-1-sulfinyl)-benzene

: 887307-88-2
(αS)-α-[1,1-dimethyl-2-[(S)-(4-methylphenyl)sulfinyl]-2-propenyl]-2-furanmethanol

Guidance literature:: methylmagnesium bromide; With copper(l) iodide; In tetrahydrofuran; at -5 ℃; for 0.75h;

1-Methyl-4-((S)-prop-1-yne-1-sulfinyl)-benzene; In tetrahydrofuran; at -30 ℃;

furfural; diiodomethane; With diethylzinc; In tetrahydrofuran; hexane; at -30 ℃;
DOI:10.1021/ja060498q

Reference yield:

: 1517-82-4
(1R,2S,5R,SS)-(-)-menthyl p-toluenesulfinate

: 887307-88-2
(αS)-α-[1,1-dimethyl-2-[(S)-(4-methylphenyl)sulfinyl]-2-propenyl]-2-furanmethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene; diethyl ether / -20 °C

2.1: CuI / tetrahydrofuran / 0.75 h / -5 °C

2.2: tetrahydrofuran / -30 °C

2.3: 75 percent / ZnEt₂ / tetrahydrofuran; hexane / -30 °C

With copper(l) iodide; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1021/ja060498q