(5-ethylnyl-2-((2-(2-(2-methoxyethoxy)ethoxy)benzyl)oxy)-1,3-phenylene)dimethanol

Base Information

Chemical Name:(5-ethylnyl-2-((2-(2-(2-methoxyethoxy)ethoxy)benzyl)oxy)-1,3-phenylene)dimethanol
CAS No.:1485487-62-4
Molecular Formula:C₂₂H₂₆O₆
Molecular Weight:386.445
Hs Code.:

Synonyms:(5-ethylnyl-2-((2-(2-(2-methoxyethoxy)ethoxy)benzyl)oxy)-1,3-phenylene)dimethanol

Suppliers and Price of (5-ethylnyl-2-((2-(2-(2-methoxyethoxy)ethoxy)benzyl)oxy)-1,3-phenylene)dimethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (5-ethylnyl-2-((2-(2-(2-methoxyethoxy)ethoxy)benzyl)oxy)-1,3-phenylene)dimethanol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (5-ethylnyl-2-((2-(2-(2-methoxyethoxy)ethoxy)benzyl)oxy)-1,3-phenylene)dimethanol

There total 10 articles about (5-ethylnyl-2-((2-(2-(2-methoxyethoxy)ethoxy)benzyl)oxy)-1,3-phenylene)dimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1252783-31-5
4-hydroxy-3,5-bis(hydroxymethyl)phenylacetylene

: 1342540-00-4
1-(bromomethyl)-2-(2-(2-methoxyethoxy)ethoxy)benzene

: 1485487-62-4
(5-ethylnyl-2-((2-(2-(2-methoxyethoxy)ethoxy)benzyl)oxy)-1,3-phenylene)dimethanol

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetone; at 0 ℃; for 40h; Reflux;
DOI:10.1246/cl.130372

Reference yield:

: 6296-63-5
4-bromo-2,6-bis(hydroxymethyl)phenol

: 1485487-62-4
(5-ethylnyl-2-((2-(2-(2-methoxyethoxy)ethoxy)benzyl)oxy)-1,3-phenylene)dimethanol

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 1.5 h / 0 - 20 °C

2: triphenylphosphine; copper(l) iodide; triethylamine / 24 h / Reflux

3: lithium hydride / tetrahydrofuran / 2 h / 0 - 20 °C

4: hydrogenchloride; water

5: potassium carbonate; 18-crown-6 ether / acetone / 40 h / 0 °C / Reflux

With hydrogenchloride; copper(l) iodide; 18-crown-6 ether; water; lithium hydride; potassium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; pyridine; acetone;
DOI:10.1246/cl.130372

Reference yield:

: 263160-70-9
1-acetoxy-2,6-bis(acetoxymethyl)-4-bromobenzene

: 1485487-62-4
(5-ethylnyl-2-((2-(2-(2-methoxyethoxy)ethoxy)benzyl)oxy)-1,3-phenylene)dimethanol

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine; copper(l) iodide; triethylamine / 24 h / Reflux

2: lithium hydride / tetrahydrofuran / 2 h / 0 - 20 °C

3: hydrogenchloride; water

4: potassium carbonate; 18-crown-6 ether / acetone / 40 h / 0 °C / Reflux

With hydrogenchloride; copper(l) iodide; 18-crown-6 ether; water; lithium hydride; potassium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; acetone;
DOI:10.1246/cl.130372