C₁₀H₁₄O₃

Base Information

Chemical Name:C₁₀H₁₄O₃
CAS No.:1256783-13-7
Molecular Formula:C₁₀H₁₄O₃
Molecular Weight:182.219
Hs Code.:

C<sub>10</sub>H<sub>14</sub>O<sub>3</sub>

Synonyms:C₁₀H₁₄O₃

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Chemical Property of C₁₀H₁₄O₃

Chemical Property:

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Technology Process of C₁₀H₁₄O₃

There total 6 articles about C₁₀H₁₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 73374-47-7
2,2-dimethyl-3-cyclohexen-1-one

: 616-38-6
carbonic acid dimethyl ester

: 1256783-13-7
C₁₀H₁₄O₃

Guidance literature:: 2,2-dimethyl-3-cyclohexen-1-one; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 1.16667h; Inert atmosphere;

carbonic acid dimethyl ester; In tetrahydrofuran; mineral oil; at 0 ℃; for 4.5h; Inert atmosphere; Reflux;

With hydrogenchloride; water; In tetrahydrofuran; mineral oil; at 0 ℃; pH=6 - 7; Inert atmosphere;
DOI:10.1021/ja108907x

Reference yield:

: 562-13-0
2,2-dimethyl-1,3-cyclohexanedione

: 1256783-13-7
C₁₀H₁₄O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene-4-sulfonic acid / dichloromethane; water / 7 h / Reflux; Inert atmosphere

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.15 h / 0 °C / Inert atmosphere

3.1: pyridine / 0 - 20 °C / Inert atmosphere

4.1: sodium ethanolate / ethanol / 48 h / Inert atmosphere; Reflux

5.1: toluene-4-sulfonic acid / acetone / 4 h / 0 - 20 °C / Inert atmosphere

6.1: sodium hydride / mineral oil; tetrahydrofuran / 1.25 h / 0 °C / Inert atmosphere

6.2: 4.5 h / 0 °C / Inert atmosphere; Reflux

With pyridine; lithium aluminium tetrahydride; sodium ethanolate; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; dichloromethane; water; acetone; mineral oil;
DOI:10.1002/asia.201403228

Reference yield:

: C₂₀H₃₀O₅S

: 1256783-13-7
C₁₀H₁₄O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium ethanolate / ethanol / 48 h / Inert atmosphere; Reflux

2.1: toluene-4-sulfonic acid / acetone / 4 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydride / mineral oil; tetrahydrofuran / 1.25 h / 0 °C / Inert atmosphere

3.2: 4.5 h / 0 °C / Inert atmosphere; Reflux

With sodium ethanolate; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; acetone; mineral oil;
DOI:10.1002/asia.201403228