4-(2,5-Dimethoxy-3,4,6-trimethylphenyl)-2-oxobutansaeure-<(1S)-1-(benzylcarbamoyl)-ethyl>ester

Base Information

Chemical Name:4-(2,5-Dimethoxy-3,4,6-trimethylphenyl)-2-oxobutansaeure-<(1S)-1-(benzylcarbamoyl)-ethyl>ester
CAS No.:103808-44-2
Molecular Formula:C₂₅H₃₁NO₆
Molecular Weight:441.524
Hs Code.:

Synonyms:4-(2,5-Dimethoxy-3,4,6-trimethylphenyl)-2-oxobutansaeure-<(1S)-1-(benzylcarbamoyl)-ethyl>ester

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Chemical Property of 4-(2,5-Dimethoxy-3,4,6-trimethylphenyl)-2-oxobutansaeure-<(1S)-1-(benzylcarbamoyl)-ethyl>ester

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Technology Process of 4-(2,5-Dimethoxy-3,4,6-trimethylphenyl)-2-oxobutansaeure-<(1S)-1-(benzylcarbamoyl)-ethyl>ester

There total 4 articles about 4-(2,5-Dimethoxy-3,4,6-trimethylphenyl)-2-oxobutansaeure-<(1S)-1-(benzylcarbamoyl)-ethyl>ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103808-42-0
2,5-dimethoxy-3,4,6-trimethylbenzaldehyde

: 103808-44-2
4-(2,5-Dimethoxy-3,4,6-trimethylphenyl)-2-oxobutansaeure-<(1S)-1-(benzylcarbamoyl)-ethyl>ester

Guidance literature:: Multi-step reaction with 4 steps

1: 4.9 g / KOH / methanol / 5 h / Heating

2: 0.75 g / 1N NaOH, H₂ / 5percent Pd/C / H₂O / 760 Torr

3: SOCl₂, pyridine

With pyridine; potassium hydroxide; sodium hydroxide; thionyl chloride; hydrogen; palladium on activated charcoal; In methanol; water;
DOI:10.1002/hlca.19900730431

Reference yield:

: 130627-46-2
4-(2,5-Dimethoxy-3,4,6-trimethylphenyl)-2-oxobut-3-ensaeure

: 103808-44-2
4-(2,5-Dimethoxy-3,4,6-trimethylphenyl)-2-oxobutansaeure-<(1S)-1-(benzylcarbamoyl)-ethyl>ester

Guidance literature:: Multi-step reaction with 3 steps

1: 0.75 g / 1N NaOH, H₂ / 5percent Pd/C / H₂O / 760 Torr

2: SOCl₂, pyridine

With pyridine; sodium hydroxide; thionyl chloride; hydrogen; palladium on activated charcoal; In water;
DOI:10.1002/hlca.19900730431

Reference yield:

: 103808-41-9
4-(2,5-Dimethoxy-3,4,6-trimethylphenyl)-2-oxobutansaeure

: 103808-44-2
4-(2,5-Dimethoxy-3,4,6-trimethylphenyl)-2-oxobutansaeure-<(1S)-1-(benzylcarbamoyl)-ethyl>ester

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂, pyridine

With pyridine; thionyl chloride;
DOI:10.1002/hlca.19900730431