(C₅Me₅)2Th(NC(Me)(3,4,5-F₃-C₆H₂))2

Base Information

Chemical Name:(C₅Me₅)2Th(NC(Me)(3,4,5-F₃-C₆H₂))2
CAS No.:937037-12-2
Molecular Formula:C₃₆H₄₀F₆N₂Th
Molecular Weight:846.756
Hs Code.:

(C<sub>5</sub>Me<sub>5</sub>)2Th(NC(Me)(3,4,5-F<sub>3</sub>-C<sub>6</sub>H<sub>2</sub>))2

Synonyms:(C₅Me₅)2Th(NC(Me)(3,4,5-F₃-C₆H₂))2

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Chemical Property of (C₅Me₅)2Th(NC(Me)(3,4,5-F₃-C₆H₂))2

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Technology Process of (C₅Me₅)2Th(NC(Me)(3,4,5-F₃-C₆H₂))2

There total 1 articles about (C₅Me₅)2Th(NC(Me)(3,4,5-F₃-C₆H₂))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 67506-90-5
dimethylbis(η5-pentamethylcyclopentadienyl)thorium

: 134227-45-5
3,4,5-trifluorobenzonitrile

: 937037-12-2
(C₅Me₅)2Th(NC(Me)(3,4,5-F₃-C₆H₂))2

Guidance literature:: In toluene; dropwise addn. of soln. of nitrile in toluene to a stirred soln. of (C5Me5)2ThMe2 in toluene under inert atmosphere, stirring at room temp. for 14 h; removal of volatiles in vac., dissolution in pentane, hot filtration through Celite, isolation of product from filtrate, drying under reduced pressure;
DOI:10.1021/ja0686458