Thorium, dimethylbis((1,2,3,4,5-eta)-1,2,3,4,5-pentamethyl-2,4-cyclopentadien-1-yl)-

Base Information

Chemical Name:Thorium, dimethylbis((1,2,3,4,5-eta)-1,2,3,4,5-pentamethyl-2,4-cyclopentadien-1-yl)-
CAS No.:67506-90-5
Molecular Formula:C22H36Th-12
Molecular Weight:532.566
Hs Code.:

Synonyms:Thorium, dimethylbis((1,2,3,4,5-eta)-1,2,3,4,5-pentamethyl-2,4-cyclopentadien-1-yl)-;Thorium, dimethylbis[(1,2,3,4,5-.eta.)-1,2,3,4,5-pentamethyl-2,4-cyclopentadien-1-yl]-;67506-90-5

Suppliers and Price of Thorium, dimethylbis((1,2,3,4,5-eta)-1,2,3,4,5-pentamethyl-2,4-cyclopentadien-1-yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Thorium, dimethylbis((1,2,3,4,5-eta)-1,2,3,4,5-pentamethyl-2,4-cyclopentadien-1-yl)-

Chemical Property:

PSA：0.00000
LogP:8.44660
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:0
Exact Mass:532.31975
Heavy Atom Count:23
Complexity:258

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:[CH3-].[CH3-].C[C-]1[C-]([C-]([C-]([C-]1C)C)C)C.C[C-]1C(=C(C(=C1C)C)C)C.[Th]

Technology Process of Thorium, dimethylbis((1,2,3,4,5-eta)-1,2,3,4,5-pentamethyl-2,4-cyclopentadien-1-yl)-

There total 3 articles about Thorium, dimethylbis((1,2,3,4,5-eta)-1,2,3,4,5-pentamethyl-2,4-cyclopentadien-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 156956-33-1
(C₅(CH₃)5)2Th(C₆H₄OCH₃)Cl

: 156956-34-2
(C₅(CH₃)5)2Th(C₆H₄OCH₃)Br

: 676-58-4
methylmagnesium chloride

: 67506-90-5
dimethylbis(η5-pentamethylcyclopentadienyl)thorium

: 156956-30-8
(C₅(CH₃)5)2Th(C₆H₄OCH₃)CH₃

Guidance literature:: With 1,4-dioxane; In toluene; under He; a soln. of MeMgCl was added to a soln. of Th complexes in toluene, p-dioxane was added, stirred for 45 min; solvent was removed in vac., extd. with toluene, filtered, removal of the solvent under reduced pressure, recrystd. from ether or toluene; elem. anal.;
DOI:10.1021/om00021a023

Reference yield: 80.0%

: 156956-37-5
(C₅(CH₃)5)2Th(C₆H₃(CH₃)2)Br

: 156956-36-4
(C₅(CH₃)5)2Th(C₆H₃(CH₃)2)Cl

: 676-58-4
methylmagnesium chloride

: 67506-90-5
dimethylbis(η5-pentamethylcyclopentadienyl)thorium

: 156956-32-0
(C₅(CH₃)5)2Th(C₆H₃(CH₃)2)CH₃

Guidance literature:: With 1,4-dioxane; In toluene; under He; a soln. of MeMgCl was added to a soln. of Th complex in toluene, p-dioxane was added, stirred for 45 min; solvent was removed in vac., extd. with toluene, filtered, removal of the solvent under reduced pressure, recrystd. from hexane at -40°C; elem. anal.;
DOI:10.1021/om00021a023

Reference yield: 66.0%

: 156956-35-3
(C₅(CH₃)5)2Th(C₆H₄(CH₃))Cl

: 676-58-4
methylmagnesium chloride

: 67506-90-5
dimethylbis(η5-pentamethylcyclopentadienyl)thorium

: 156956-31-9
(C₅(CH₃)5)2Th(C₆H₄CH₃)CH₃

Guidance literature:: With 1,4-dioxane; In toluene; under He; a soln. of MeMgCl was added to a soln. of Th complex in toluene, p-dioxane was added, stirred for 45 min; solvent was removed in vac., extd. with toluene, filtered, removal of the solvent under reduced pressure, recrystd. from hexane at -40°C; elem. anal.;
DOI:10.1021/om00021a023