N-((1-benzylcyclopropyl)methyl)-N-(2-bromophenyl)-1,1,1-trifluoromethanesulfonamide

Base Information

Chemical Name:N-((1-benzylcyclopropyl)methyl)-N-(2-bromophenyl)-1,1,1-trifluoromethanesulfonamide
CAS No.:1448600-02-9
Molecular Formula:C₁₈H₁₇BrF₃NO₂S
Molecular Weight:448.304
Hs Code.:

Synonyms:N-((1-benzylcyclopropyl)methyl)-N-(2-bromophenyl)-1,1,1-trifluoromethanesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((1-benzylcyclopropyl)methyl)-N-(2-bromophenyl)-1,1,1-trifluoromethanesulfonamide

Chemical Property:

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Technology Process of N-((1-benzylcyclopropyl)methyl)-N-(2-bromophenyl)-1,1,1-trifluoromethanesulfonamide

There total 4 articles about N-((1-benzylcyclopropyl)methyl)-N-(2-bromophenyl)-1,1,1-trifluoromethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 1448600-56-3
C₁₇H₁₈BrN

: 1448600-02-9
N-((1-benzylcyclopropyl)methyl)-N-(2-bromophenyl)-1,1,1-trifluoromethanesulfonamide

Guidance literature:: With sodium hydride; In 1,2-dichloro-ethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201207959

Reference yield:

: 27356-91-8
1-benzylcyclopropanecarboxylic acid

: 1448600-02-9
N-((1-benzylcyclopropyl)methyl)-N-(2-bromophenyl)-1,1,1-trifluoromethanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: borane-THF / tetrahydrofuran / 8 h / Reflux; Inert atmosphere

4.1: sodium hydride / 1,2-dichloro-ethane / 0 - 20 °C / Inert atmosphere

With borane-THF; oxalyl dichloride; sodium hydride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/anie.201207959

Reference yield:

: 105676-90-2
1-Benzylcyclopropancarbonylchlorid

: 1448600-02-9
N-((1-benzylcyclopropyl)methyl)-N-(2-bromophenyl)-1,1,1-trifluoromethanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: borane-THF / tetrahydrofuran / 8 h / Reflux; Inert atmosphere

3.1: sodium hydride / 1,2-dichloro-ethane / 0 - 20 °C / Inert atmosphere

With borane-THF; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/anie.201207959