tri-tert-butyl 2,2',2''-(((10-(2-((4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)carbamoyl)phenyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate

Base Information

Chemical Name:tri-tert-butyl 2,2',2''-(((10-(2-((4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)carbamoyl)phenyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate
CAS No.:1509916-07-7
Molecular Formula:C₄₉H₆₇N₇O₉S
Molecular Weight:930.178
Hs Code.:

tri-tert-butyl 2,2',2''-(((10-(2-((4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)carbamoyl)phenyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate

Synonyms:tri-tert-butyl 2,2',2''-(((10-(2-((4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)carbamoyl)phenyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate

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Chemical Property of tri-tert-butyl 2,2',2''-(((10-(2-((4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)carbamoyl)phenyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate

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Technology Process of tri-tert-butyl 2,2',2''-(((10-(2-((4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)carbamoyl)phenyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate

There total 9 articles about tri-tert-butyl 2,2',2''-(((10-(2-((4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)carbamoyl)phenyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1509916-06-6
4-(2-chloroacetamido)-N-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)benzamide

: 122555-91-3
1,4,7-tris-tert-butoxycarbonylmethyl-1,4,7,10-tetraazacyclododecane

: 1509916-07-7
tri-tert-butyl 2,2',2''-(((10-(2-((4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)carbamoyl)phenyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 48h;
DOI:10.1007/s00775-013-1055-8

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1509916-07-7
tri-tert-butyl 2,2',2''-(((10-(2-((4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)carbamoyl)phenyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / tetrahydrofuran / -0.16 °C

2: Lawessons reagent / chlorobenzene / Reflux

3: sodium hydroxide; potassium hexacyanoferrate(III) / Reflux

4: tin(ll) chloride / ethanol / Reflux

5: potassium carbonate / acetone

6: potassium carbonate / acetonitrile / 48 h / 20 °C

With Lawessons reagent; potassium carbonate; triethylamine; tin(ll) chloride; sodium hydroxide; potassium hexacyanoferrate(III); In tetrahydrofuran; ethanol; chlorobenzene; acetone; acetonitrile;
DOI:10.1007/s00775-013-1055-8

Reference yield:

: 24730-11-8
N-(4-methoxyphenyl)-4-nitrobenzamide

: 1509916-07-7
tri-tert-butyl 2,2',2''-(((10-(2-((4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)carbamoyl)phenyl)amino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate

Guidance literature:: Multi-step reaction with 5 steps

1: Lawessons reagent / chlorobenzene / Reflux

2: sodium hydroxide; potassium hexacyanoferrate(III) / Reflux

3: tin(ll) chloride / ethanol / Reflux

4: potassium carbonate / acetone

5: potassium carbonate / acetonitrile / 48 h / 20 °C

With Lawessons reagent; potassium carbonate; tin(ll) chloride; sodium hydroxide; potassium hexacyanoferrate(III); In ethanol; chlorobenzene; acetone; acetonitrile;
DOI:10.1007/s00775-013-1055-8