benzyl 5-amino-3,4-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid

Base Information

• Chemical Name: benzyl 5-amino-3,4-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid
• CAS No.: 101554-19-2
• Molecular Formula: C₁₆H₂₃NO₈
• Molecular Weight: 357.361

Synonyms:benzyl 5-amino-3,4-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid

Chemical Property of benzyl 5-amino-3,4-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid

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Technology Process of benzyl 5-amino-3,4-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid

There total 6 articles about benzyl 5-amino-3,4-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

sodium (benzyl 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosid)onate → benzyl 5-amino-3,4-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid (101554-19-2)

Guidance literature:

With sodium hydroxide; at 110 ℃; for 10h;

DOI:10.1016/S0008-6215(92)84240-S

Reference yield: 85.0%

methyl (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranosid)onate (19342-75-7) → benzyl 5-amino-3,4-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid (101554-19-2)

Guidance literature:

With sodium hydroxide; for 6h; Heating;

DOI:10.1016/j.carres.2004.05.028

Reference yield: 62.0%

Neu5AcαOBn (14206-38-3) → benzyl 5-amino-3,4-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranosidonic acid (101554-19-2)

Guidance literature:

With barium dihydroxide; at 90 ℃; for 10h;

DOI:10.1248/cpb.43.1844

upstream raw materials:

Neu5AcαOBn

methyl (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-α-D-glycero-D-galacto-2-nonulopyranosid)onate

(1S,2R)-1-((2R,3R,4S,6R)-3-acetamido-4,6-diacetoxy-6-(methoxycarbonyl)tetrahydro-2H-pyran-2-yl)propane-1,2,3-triyl triacetate

methyl 5-acetamido-2,4,7,8,9-penta-O-acetyl-3,5-dideoxy-D-glycero-D-galacto-2-nonulopyranosonate

Downstream raw materials:

(2R,4S,5R,6R)-5-(2-Acetoxy-acetylamino)-2-benzyloxy-4-hydroxy-6-((1R,2R)-1,2,3-trihydroxy-propyl)-tetrahydro-pyran-2-carboxylic acid

N-phenylacetyl-D-neuraminic acid benzyl glycoside

N-iso-butanoyl-D-neuraminic acid benzyl glycoside

N-propionyl-D-neuraminic acid benzyl glycoside

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