ethyl 2-[3-(tert-butyldiphenylsilanyloxy)propyl]cycloprop-2-enecarboxylate

Base Information

Chemical Name:ethyl 2-[3-(tert-butyldiphenylsilanyloxy)propyl]cycloprop-2-enecarboxylate
CAS No.:1202871-38-2
Molecular Formula:C₂₅H₃₂O₃Si
Molecular Weight:408.613
Hs Code.:

Synonyms:ethyl 2-[3-(tert-butyldiphenylsilanyloxy)propyl]cycloprop-2-enecarboxylate

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Chemical Property of ethyl 2-[3-(tert-butyldiphenylsilanyloxy)propyl]cycloprop-2-enecarboxylate

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Technology Process of ethyl 2-[3-(tert-butyldiphenylsilanyloxy)propyl]cycloprop-2-enecarboxylate

There total 1 articles about ethyl 2-[3-(tert-butyldiphenylsilanyloxy)propyl]cycloprop-2-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 623-73-4
diazoacetic acid ethyl ester

: 91266-03-4
tert-butyl-pent-4-ynyloxy-diphenyl-silane

: 1202871-38-2
ethyl 2-[3-(tert-butyldiphenylsilanyloxy)propyl]cycloprop-2-enecarboxylate

Guidance literature:: With dirhodium tetraacetate; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1021/acs.orglett.1c01840

Reference yield: 87.0%

: 1202871-38-2
ethyl 2-[3-(tert-butyldiphenylsilanyloxy)propyl]cycloprop-2-enecarboxylate

: 1202871-41-7
{2-[3-(tert-butyldiphenylsilanyloxy)propyl]cycloprop-2-enyl}methanol

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at -78 ℃; for 0.5h;
DOI:10.1021/acs.orglett.1c01840

Reference yield: 66.0%

: 1202871-38-2
ethyl 2-[3-(tert-butyldiphenylsilanyloxy)propyl]cycloprop-2-enecarboxylate

: 1202871-39-3
2-[3-(tert-butyldiphenylsilanyloxy)propyl]cycloprop-2-enecarboxylic acid

Guidance literature:: ethyl 2-[3-(tert-butyldiphenylsilanyloxy)propyl]cycloprop-2-enecarboxylate; With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃;

With hydrogenchloride; In diethyl ether; water; pH=1;
DOI:10.1021/ol9025606