{3-[5-(5-isopropyl-2,4-bis-methoxymethoxy-phenyl)-4-isopropyl-4H-[1,2,4]triazol-3-ylsulfanyl]-propyl}-dimethylamine

Base Information

Chemical Name:{3-[5-(5-isopropyl-2,4-bis-methoxymethoxy-phenyl)-4-isopropyl-4H-[1,2,4]triazol-3-ylsulfanyl]-propyl}-dimethylamine
CAS No.:909872-91-9
Molecular Formula:C₂₃H₃₈N₄O₄S
Molecular Weight:466.645
Hs Code.:

Synonyms:{3-[5-(5-isopropyl-2,4-bis-methoxymethoxy-phenyl)-4-isopropyl-4H-[1,2,4]triazol-3-ylsulfanyl]-propyl}-dimethylamine

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Chemical Property of {3-[5-(5-isopropyl-2,4-bis-methoxymethoxy-phenyl)-4-isopropyl-4H-[1,2,4]triazol-3-ylsulfanyl]-propyl}-dimethylamine

Chemical Property:

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Technology Process of {3-[5-(5-isopropyl-2,4-bis-methoxymethoxy-phenyl)-4-isopropyl-4H-[1,2,4]triazol-3-ylsulfanyl]-propyl}-dimethylamine

There total 6 articles about {3-[5-(5-isopropyl-2,4-bis-methoxymethoxy-phenyl)-4-isopropyl-4H-[1,2,4]triazol-3-ylsulfanyl]-propyl}-dimethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 909871-30-3
5-(5-isopropyl-2,4-bismethoxymethoxy-phenyl)-4-isopropyl-2,3-dihydro-4H-[1,2,4]triazol-3-thion

: 5407-04-5
3-(dimethylamino)propyl chloride hydrochloride

: 909872-91-9
{3-[5-(5-isopropyl-2,4-bis-methoxymethoxy-phenyl)-4-isopropyl-4H-[1,2,4]triazol-3-ylsulfanyl]-propyl}-dimethylamine

Guidance literature:: With potassium carbonate; In ethanol; at 100 ℃; for 1h;

Reference yield:

: 909870-97-9
4-bromo-6-isopropyl-benzene-1,3-diol

: 909872-91-9
{3-[5-(5-isopropyl-2,4-bis-methoxymethoxy-phenyl)-4-isopropyl-4H-[1,2,4]triazol-3-ylsulfanyl]-propyl}-dimethylamine

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18.5 h / 20 - 50 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -60 - -40 °C

2.2: -40 - 20 °C

3.1: 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / N,N-dimethyl-formamide / 3 h / 20 °C

3.2: 1 h

4.1: potassium hydroxide / ethanol; water / 13 h / 90 °C

5.1: potassium carbonate / ethanol / 1 h / 100 °C

With potassium hydroxide; n-butyllithium; potassium carbonate; N-ethyl-N,N-diisopropylamine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In tetrahydrofuran; ethanol; hexane; water; N,N-dimethyl-formamide;

Reference yield:

: 909870-98-0
1-bromo-5-isopropyl-2,4-bis-methoxymethoxy-benzene

: 909872-91-9
{3-[5-(5-isopropyl-2,4-bis-methoxymethoxy-phenyl)-4-isopropyl-4H-[1,2,4]triazol-3-ylsulfanyl]-propyl}-dimethylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -60 - -40 °C

1.2: -40 - 20 °C

2.1: 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride / N,N-dimethyl-formamide / 3 h / 20 °C

2.2: 1 h

3.1: potassium hydroxide / ethanol; water / 13 h / 90 °C

4.1: potassium carbonate / ethanol / 1 h / 100 °C

With potassium hydroxide; n-butyllithium; potassium carbonate; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In tetrahydrofuran; ethanol; hexane; water; N,N-dimethyl-formamide;