5-[({4-[3-(2-cyclohexylethoxy)benzoyl]piperazin-1-yl}carbonyl)amino]-1,3-phenylene diacetate

Base Information

Chemical Name:5-[({4-[3-(2-cyclohexylethoxy)benzoyl]piperazin-1-yl}carbonyl)amino]-1,3-phenylene diacetate
CAS No.:1008775-29-8
Molecular Formula:C₃₀H₃₇N₃O₇
Molecular Weight:551.64
Hs Code.:

Synonyms:5-[({4-[3-(2-cyclohexylethoxy)benzoyl]piperazin-1-yl}carbonyl)amino]-1,3-phenylene diacetate

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Chemical Property of 5-[({4-[3-(2-cyclohexylethoxy)benzoyl]piperazin-1-yl}carbonyl)amino]-1,3-phenylene diacetate

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Technology Process of 5-[({4-[3-(2-cyclohexylethoxy)benzoyl]piperazin-1-yl}carbonyl)amino]-1,3-phenylene diacetate

There total 3 articles about 5-[({4-[3-(2-cyclohexylethoxy)benzoyl]piperazin-1-yl}carbonyl)amino]-1,3-phenylene diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1008774-26-2
1-[3-(2-cyclohexylethoxy)benzoyl]piperazine hydrochloride

: C₁₁H₉NO₅

: 1008775-29-8
5-[({4-[3-(2-cyclohexylethoxy)benzoyl]piperazin-1-yl}carbonyl)amino]-1,3-phenylene diacetate

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 2h;

Reference yield:

: C₁₁H₉N₃O₅

: 1008775-29-8
5-[({4-[3-(2-cyclohexylethoxy)benzoyl]piperazin-1-yl}carbonyl)amino]-1,3-phenylene diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 4 h / 100 °C

2: triethylamine / acetonitrile / 2 h / 20 °C

With triethylamine; In toluene; acetonitrile;

Reference yield:

: 35354-29-1
3,5-diacetoxybenzoic acid

: 1008775-29-8
5-[({4-[3-(2-cyclohexylethoxy)benzoyl]piperazin-1-yl}carbonyl)amino]-1,3-phenylene diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: diphenyl phosphoryl azide; triethylamine / toluene / 3 h

2: toluene / 4 h / 100 °C

3: triethylamine / acetonitrile / 2 h / 20 °C

With diphenyl phosphoryl azide; triethylamine; In toluene; acetonitrile;