2-(1-benzyl-5-methoxy-1H-indol-3-yl)-ethylamine; hydrochloride

Base Information

• Chemical Name: 2-(1-benzyl-5-methoxy-1H-indol-3-yl)-ethylamine; hydrochloride
• CAS No.: 1947-81-5
• Molecular Formula: C₁₈H₂₀N₂O*ClH
• Molecular Weight: 316.831

Synonyms:2-(1-benzyl-5-methoxy-1H-indol-3-yl)-ethylamine; hydrochloride

Chemical Property of 2-(1-benzyl-5-methoxy-1H-indol-3-yl)-ethylamine; hydrochloride

Chemical Property:

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Technology Process of 2-(1-benzyl-5-methoxy-1H-indol-3-yl)-ethylamine; hydrochloride

There total 1 articles about 2-(1-benzyl-5-methoxy-1H-indol-3-yl)-ethylamine; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C23H28N2O3 (1159000-22-2) → 2-(1-benzyl-5-methoxy-1H-indol-3-yl)-ethylamine; hydrochloride (1947-81-5,18690-44-3)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 0 - 20 ℃;

DOI:10.1002/ejoc.200900033

Reference yield: 45.0%

2-(1-benzyl-5-methoxy-1H-indol-3-yl)-ethylamine; hydrochloride (1947-81-5,18690-44-3) + 2-[(trimethylsilanyl)ethynyl]benzoic acid (205250-12-0) → N-(2-(1-benzyl-5-methoxy-1H-indol-3-yl)ethyl)-2-ethynylbenzamide

Guidance literature:

2-[(trimethylsilanyl)ethynyl]benzoic acid; With 1,1'-carbonyldiimidazole; In dichloromethane; for 0.25h;

2-(1-benzyl-5-methoxy-1H-indol-3-yl)-ethylamine; hydrochloride; With triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;

With potassium carbonate; In methanol; for 0.5h;

DOI:10.1021/acs.orglett.8b03275

Reference yield:

2-(1-benzyl-5-methoxy-1H-indol-3-yl)-ethylamine; hydrochloride (1947-81-5,18690-44-3) + 4-[(trimethylsilyl)methyl]but-3-enoic acid (62477-64-9) → C26H34N2O2Si (1159000-24-4)

Guidance literature:

2-(1-benzyl-5-methoxy-1H-indol-3-yl)-ethylamine; hydrochloride; With benzotriazol-1-ol; In dichloromethane; at 20 ℃; for 0.0833333h;

4-[(trimethylsilyl)methyl]but-3-enoic acid; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1002/ejoc.200900033

upstream raw materials:

C₂₃H₂₈N₂O₃

Downstream raw materials:

C₂₆H₃₄N₂O₂Si

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