3,5-di-tert-butyl-1-isobutylbenzene

Base Information

• Chemical Name: 3,5-di-tert-butyl-1-isobutylbenzene
• CAS No.: 106470-71-7
• Molecular Formula: C₁₈H₃₀
• Molecular Weight: 246.436
• Mol file: 106470-71-7.mol

Synonyms:3,5-di-tert-butyl-1-isobutylbenzene

Chemical Property of 3,5-di-tert-butyl-1-isobutylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,5-di-tert-butyl-1-isobutylbenzene

There total 3 articles about 3,5-di-tert-butyl-1-isobutylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2,4,6-tri-tert-butylnitrobenzene (4074-25-3) + 9-methoxyfluorene (19126-15-9) → 1,3,5-Tri-tert-butylbenzene (1460-02-2) + 9,9'-dimethoxy-9,9'-bifluorene (50616-99-4) + 3,5-di-tert-butyl-1-isobutylbenzene (106470-71-7)

Guidance literature:

With carbonic-acid; potassium tert-butylate; In tetrahydrofuran; at 50 ℃; for 48h; Product distribution; other sterically protected nitroarene; other strong basis;

DOI:10.1021/jo00381a005

Reference yield:

1-bromo-2,4,6-tri-tert-butylbenzene (3975-77-7) → 1,3,5-Tri-tert-butylbenzene (1460-02-2) + 3,5-di-tert-butyl-1-isobutylbenzene (106470-71-7)

Guidance literature:

With potassium tert-butylate; sodium hydride; benzene; at 150 ℃; for 21h; Temperature; Reagent/catalyst; Inert atmosphere; Sealed tube;

DOI:10.1021/jacs.8b07632

Reference yield:

1,3,5-Tri-tert-butylbenzene (1460-02-2) → 3,5-di-tert-butyl-1-isobutylbenzene (106470-71-7)

Guidance literature:

With di-tert-butylbenzene; at 150 ℃; for 19h;

DOI:10.1021/jo00381a005

upstream raw materials:

1,3,5-Tri-tert-butylbenzene

2,4,6-tri-tert-butylnitrobenzene

9-methoxyfluorene

1-bromo-2,4,6-tri-tert-butylbenzene