((S)-4-(4-(2-(methylamino)benzamido)butanamido)cyclopent-1-en-1-yl)(butyl)phosphinic acid

Base Information

Chemical Name:((S)-4-(4-(2-(methylamino)benzamido)butanamido)cyclopent-1-en-1-yl)(butyl)phosphinic acid
CAS No.:1425330-68-2
Molecular Formula:C₂₁H₃₂N₃O₄P
Molecular Weight:421.477
Hs Code.:

Synonyms:((S)-4-(4-(2-(methylamino)benzamido)butanamido)cyclopent-1-en-1-yl)(butyl)phosphinic acid

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Chemical Property of ((S)-4-(4-(2-(methylamino)benzamido)butanamido)cyclopent-1-en-1-yl)(butyl)phosphinic acid

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Technology Process of ((S)-4-(4-(2-(methylamino)benzamido)butanamido)cyclopent-1-en-1-yl)(butyl)phosphinic acid

There total 3 articles about ((S)-4-(4-(2-(methylamino)benzamido)butanamido)cyclopent-1-en-1-yl)(butyl)phosphinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1425330-52-4
((S)-4-(4-aminobutanamido)cyclopent-1-en-1-yl)(butyl)phosphinic acid

: 64156-72-5
2-methylaminobenzoic acid 2,5-dioxopyrrolidin-1-yl ester

: 1425330-68-2
((S)-4-(4-(2-(methylamino)benzamido)butanamido)cyclopent-1-en-1-yl)(butyl)phosphinic acid

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; 1,2-dimethoxyethane; water; at 20 ℃; for 16h;
DOI:10.1021/ml300476v

Reference yield:

: 119-68-6
N-Methylanthranilic acid

: 1425330-68-2
((S)-4-(4-(2-(methylamino)benzamido)butanamido)cyclopent-1-en-1-yl)(butyl)phosphinic acid

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

2: sodium hydrogencarbonate / water; 1,2-dimethoxyethane; tetrahydrofuran / 16 h / 20 °C

With dmap; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1021/ml300476v

Reference yield:

: 1425330-84-2
((S)-4-(4-((tert-butoxycarbonyl)amino)butanamido)cyclopent-1-en-1-yl)(butyl)phosphinic acid

: 1425330-68-2
((S)-4-(4-(2-(methylamino)benzamido)butanamido)cyclopent-1-en-1-yl)(butyl)phosphinic acid

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 20 °C

2: sodium hydrogencarbonate / water; 1,2-dimethoxyethane; tetrahydrofuran / 16 h / 20 °C

With sodium hydrogencarbonate; trifluoroacetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1021/ml300476v