4-Nitro-benzoic acid (2S,3S)-3-[2-((R)-3,3-dimethyl-oxiranyl)-ethyl]-3-methyl-oxiranylmethyl ester

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Chemical Name:4-Nitro-benzoic acid (2S,3S)-3-[2-((R)-3,3-dimethyl-oxiranyl)-ethyl]-3-methyl-oxiranylmethyl ester
CAS No.:146204-97-9
Molecular Formula:C₁₇H₂₁NO₆
Molecular Weight:335.357
Hs Code.:

Synonyms:4-Nitro-benzoic acid (2S,3S)-3-[2-((R)-3,3-dimethyl-oxiranyl)-ethyl]-3-methyl-oxiranylmethyl ester

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Chemical Property of 4-Nitro-benzoic acid (2S,3S)-3-[2-((R)-3,3-dimethyl-oxiranyl)-ethyl]-3-methyl-oxiranylmethyl ester

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Technology Process of 4-Nitro-benzoic acid (2S,3S)-3-[2-((R)-3,3-dimethyl-oxiranyl)-ethyl]-3-methyl-oxiranylmethyl ester

There total 5 articles about 4-Nitro-benzoic acid (2S,3S)-3-[2-((R)-3,3-dimethyl-oxiranyl)-ethyl]-3-methyl-oxiranylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 146204-96-8
4-Nitro-benzoic acid (2S,3S)-3-((S)-3-bromo-4-hydroxy-4-methyl-pentyl)-3-methyl-oxiranylmethyl ester

: 146204-97-9
4-Nitro-benzoic acid (2S,3S)-3-[2-((R)-3,3-dimethyl-oxiranyl)-ethyl]-3-methyl-oxiranylmethyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene;
DOI:10.1016/S0040-4039(00)74741-1

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 146338-69-4
{(2S,3S)-3-[2-((R)-3,3-Dimethyl-oxiranyl)-ethyl]-3-methyl-oxiranyl}-methanol

: 146204-97-9
4-Nitro-benzoic acid (2S,3S)-3-[2-((R)-3,3-dimethyl-oxiranyl)-ethyl]-3-methyl-oxiranylmethyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2013.04.041

Reference yield:

: 106-24-1
Geraniol

: 146204-97-9
4-Nitro-benzoic acid (2S,3S)-3-[2-((R)-3,3-dimethyl-oxiranyl)-ethyl]-3-methyl-oxiranylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: (+)-diethyl tartrate, TBHP / Ti(OiPr)4

2: 72 percent / NEt₃

3: N-bromosuccinimide, H₂O

4: 67 percent / 1,8-diazabicyclo<5.4.0>-7-undecene

With tert.-butylhydroperoxide; N-Bromosuccinimide; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; (+)-Weinsaeure-diethylester; triethylamine; titanium(IV) isopropylate;
DOI:10.1016/S0040-4039(00)74741-1