1-(4,5-dihydro-3,5-di-p-tolylpyrazol-1-yl)-2-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)ethanone

Base Information

Chemical Name:1-(4,5-dihydro-3,5-di-p-tolylpyrazol-1-yl)-2-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)ethanone
CAS No.:1394072-26-4
Molecular Formula:C₂₇H₂₆N₆O₂
Molecular Weight:466.542
Hs Code.:

Synonyms:1-(4,5-dihydro-3,5-di-p-tolylpyrazol-1-yl)-2-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)ethanone

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Chemical Property of 1-(4,5-dihydro-3,5-di-p-tolylpyrazol-1-yl)-2-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)ethanone

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Technology Process of 1-(4,5-dihydro-3,5-di-p-tolylpyrazol-1-yl)-2-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)ethanone

There total 6 articles about 1-(4,5-dihydro-3,5-di-p-tolylpyrazol-1-yl)-2-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.2%

: 13565-37-2
trans-4,4'-dimethylchalcone

: 1394071-86-3
2-[5-(4-methoxyphenyl)-1H-tetrazol-1-yl]acetohydrazide

: 1394072-26-4
1-(4,5-dihydro-3,5-di-p-tolylpyrazol-1-yl)-2-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)ethanone

Guidance literature:: With sodium hydroxide; In methanol; Reflux;
DOI:10.1016/j.ejmech.2012.03.049

Reference yield:

: C₁₂H₁₄N₄O₃

: 1394072-26-4
1-(4,5-dihydro-3,5-di-p-tolylpyrazol-1-yl)-2-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / Reflux

2: sodium hydroxide / methanol / Reflux

With hydrazine hydrate; sodium hydroxide; In methanol; ethanol;
DOI:10.1016/j.ejmech.2012.03.049

Reference yield:

: 3717-21-3,3717-22-4,140461-28-5,140461-29-6,3235-04-9
p-methoxyl benzaldoxime

: 1394072-26-4
1-(4,5-dihydro-3,5-di-p-tolylpyrazol-1-yl)-2-(5-(4-methoxyphenyl)-1H-tetrazol-1-yl)ethanone

Guidance literature:: Multi-step reaction with 5 steps

1: acetic anhydride / Reflux

2: sodium azide; zinc dibromide / isopropyl alcohol / 24 h / Reflux

3: potassium carbonate / acetone

4: hydrazine hydrate / ethanol / Reflux

5: sodium hydroxide / methanol / Reflux

With sodium azide; acetic anhydride; potassium carbonate; hydrazine hydrate; sodium hydroxide; zinc dibromide; In methanol; ethanol; isopropyl alcohol; acetone;
DOI:10.1016/j.ejmech.2012.03.049