GLUCOTROPAEOLIN

Base Information

• Chemical Name: GLUCOTROPAEOLIN
• CAS No.: 5115-71-9
• Molecular Formula: C14H19 N O9 S2 . K
• Molecular Weight: 447.529
• Hs Code.: 2942000090
• Mol file: 5115-71-9.mol

Synonyms:Glucopyranose,1-thio-, 1-(2-phenylacetohydroximate) NO-(hydrogen sulfate), monopotassiumsalt, b-D- (8CI); Glucopyranose,1-thio-, 1-(phenylacetate), oxime, O-sulfate, potassium salt, b-D- (7CI); Glucopyranose,1-thio-, S-phenylacetate, oxime, hydrogen sulfate, potassium salt, b-D- (6CI); Glucotropaeolin,potassium salt

Chemical Property of GLUCOTROPAEOLIN

Chemical Property:

• Melting Point: 188～189℃
• PSA: 202.62000
• LogP: -0.36670

Purity/Quality:

99%, ^*data from raw suppliers

Glucotropaeolin ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Glucotropaeolin is a phytochemical from Tropaeolum majus used in a wide range of biochemical studies.

Technology Process of GLUCOTROPAEOLIN

There total 6 articles about GLUCOTROPAEOLIN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2',3',4',6'-tetra-O-acetylglucotropaeolin potassium salt monohydrate → Glucotropaeolin potassium salt (5115-71-9)

Guidance literature:

With potassium hydroxide; In methanol; at 20 ℃; for 2h;

DOI:10.1055/s-0036-1591895

Reference yield:

Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(N-hydroxy-2-phenyl-acetimidoylsulfanyl)-tetrahydro-pyran-3-yl ester (130718-54-6) → C14H18NO9S2(1-)*K(1+) (5115-71-9,5115-72-0)

Guidance literature:

With pyridine; chlorosulfonic acid; ammonia; Multistep reaction; 1) CH₂Cl₂ 2) MeOH;

DOI:10.1016/S0040-4039(00)97490-2

Reference yield:

phenylmethanenitrile oxide (71494-99-0) → C14H18NO9S2(1-)*K(1+) (5115-71-9,5115-72-0)

Guidance literature:

Multi-step reaction with 2 steps

2: 1) ClSO₃H, pyridine 2) NH₃ / 1) CH₂Cl₂ 2) MeOH

With pyridine; chlorosulfonic acid; ammonia;

DOI:10.1016/S0040-4039(00)97490-2

upstream raw materials:

Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(N-hydroxy-2-phenyl-acetimidoylsulfanyl)-tetrahydro-pyran-3-yl ester

phenylmethanenitrile oxide

2,3,4,6-tetra-O-acetyl-1-thio-α-D-glucopyranose

1-S-trityl-2,3,4,6-tetra-O-acetyl-1-thio-α-D-glucopyranose

Downstream raw materials:

benzyl thiocyanate

C₂₉H₅₉NO₆SSi₅

D-glucose

benzylamine

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