C₁₅H₁₆⁽²⁾H₂O₄S

Base Information

Chemical Name:C₁₅H₁₆⁽²⁾H₂O₄S
CAS No.:82043-82-1
Molecular Formula:C₁₅H₁₈O₄S
Molecular Weight:296.356
Hs Code.:

C<sub>15</sub>H<sub>16</sub><sup>(2)</sup>H<sub>2</sub>O<sub>4</sub>S

Synonyms:C₁₅H₁₆⁽²⁾H₂O₄S

Suppliers and Price of C₁₅H₁₆⁽²⁾H₂O₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₆⁽²⁾H₂O₄S

Chemical Property:

Purity/Quality:

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Technology Process of C₁₅H₁₆⁽²⁾H₂O₄S

There total 5 articles about C₁₅H₁₆⁽²⁾H₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31444-18-5,802911-71-3
norbornenone ethylene glycol ketal

: 82043-82-1
C₁₅H₁₆⁽²⁾H₂O₄S

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) D₂, 2.) 2percent H₂SO₄ / 1.) 10percent Pd on charcoal / 1.) ether, 18 h, 2.) water, 1 h

2: LDA / hexane; tetrahydrofuran / 1.) -60 deg C, 5 min, 2.) -100 deg C, 3.) warm to room temperature

3: CF₃COOH / methanol / 3 h / Heating

4: Et₃N / -78 - 0 °C

5: 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 1.5 h

With sulfuric acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; deuterium; trifluoroacetic acid; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1021/ja00379a018

Reference yield:

: C₁₅H₁₆⁽²⁾H₂O₃S

: 82043-82-1
C₁₅H₁₆⁽²⁾H₂O₄S

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 1.5h;
DOI:10.1021/ja00379a018

Reference yield:

: 28956-11-8,87337-83-5,55297-86-4
5-exo,6-exo-dideuteriobicyclo<2.2.1>heptan-2-one

: 82043-82-1
C₁₅H₁₆⁽²⁾H₂O₄S

Guidance literature:: Multi-step reaction with 4 steps

1: LDA / hexane; tetrahydrofuran / 1.) -60 deg C, 5 min, 2.) -100 deg C, 3.) warm to room temperature

2: CF₃COOH / methanol / 3 h / Heating

3: Et₃N / -78 - 0 °C

4: 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 1.5 h

With triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1021/ja00379a018