norbornenone ethylene glycol ketal

Base Information

• Chemical Name: norbornenone ethylene glycol ketal
• CAS No.: 31444-18-5
• Molecular Formula: C₉H₁₂O₂
• Molecular Weight: 152.193

Synonyms:norbornenone ethylene glycol ketal

Chemical Property of norbornenone ethylene glycol ketal

Chemical Property:

• Boiling Point: 228.6±40.0 °C(Predicted)
• Density: 1.18±0.1 g/cm3(Predicted)

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of norbornenone ethylene glycol ketal

There total 12 articles about norbornenone ethylene glycol ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

5,6-bis(benzenesulfonyl)bicyclo<2.2.1.>heptan-2-one ethylene ketal (93914-95-5,133813-32-8,133813-33-9) → C9H12O2 (31444-18-5,802911-71-3)

Guidance literature:

With sodium dihydrogenphosphate; sodium amalgam; In methanol; Ambient temperature;

Reference yield: 88.1%

norborn-5-en-2-one (694-98-4) + ethylene glycol (107-21-1) → norbornenone ethylene glycol ketal (31444-18-5,802911-71-3)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; for 60h; Heating / reflux;

Reference yield: 4.0%

Spirohepta-2,2'-<1,3>dioxolan>-5-on-p-tolylsulfonylhydrazon (111292-22-9) → C9H12O2 (31444-18-5,802911-71-3) + C9H12O2 (3213-76-1) + exo-5-Methoxy-spiroheptan-2,2'-<1,3>dioxolan> (111292-24-1)

Guidance literature:

With sodium methylate; In methanol; for 4h; Irradiation;

upstream raw materials:

6-bromobicyclo<2.2.1>hept-5-en-2-one ethylene ketal

norborn-5-en-2-one

ethylene glycol

5-norbornene-2-ol

Downstream raw materials:

2-Chloro-2-[(1S,2S)-2-(2,4-dinitro-phenylsulfanyl)-cyclopent-3-enylmethyl]-[1,3]dioxolane

C₁₅H₁₆⁽²⁾H₂O₄S

C₉H₁₂O₂

Spirohepta-2,2'-<1,3>dioxolan>-5-on-p-tolylsulfonylhydrazon

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