2,4-Dimethoxy-benzoic acid (1R,3R,4R,5S,11S)-3-(2-amino-6-chloro-purin-9-yl)-7,7,9,9-tetraisopropyl-6,8,10-trioxa-2-thia-7,9-disila-tricyclo[9.3.0.0^1,5]tetradec-4-yl ester

Base Information

• Chemical Name: 2,4-Dimethoxy-benzoic acid (1R,3R,4R,5S,11S)-3-(2-amino-6-chloro-purin-9-yl)-7,7,9,9-tetraisopropyl-6,8,10-trioxa-2-thia-7,9-disila-tricyclo[9.3.0.0^1,5]tetradec-4-yl ester
• CAS No.: 862081-05-8
• Molecular Formula: C₃₄H₅₀ClN₅O₇SSi₂
• Molecular Weight: 764.49

Synonyms:2,4-Dimethoxy-benzoic acid (1R,3R,4R,5S,11S)-3-(2-amino-6-chloro-purin-9-yl)-7,7,9,9-tetraisopropyl-6,8,10-trioxa-2-thia-7,9-disila-tricyclo[9.3.0.0^1,5]tetradec-4-yl ester

Chemical Property of 2,4-Dimethoxy-benzoic acid (1R,3R,4R,5S,11S)-3-(2-amino-6-chloro-purin-9-yl)-7,7,9,9-tetraisopropyl-6,8,10-trioxa-2-thia-7,9-disila-tricyclo[9.3.0.0^1,5]tetradec-4-yl ester

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Technology Process of 2,4-Dimethoxy-benzoic acid (1R,3R,4R,5S,11S)-3-(2-amino-6-chloro-purin-9-yl)-7,7,9,9-tetraisopropyl-6,8,10-trioxa-2-thia-7,9-disila-tricyclo[9.3.0.0^1,5]tetradec-4-yl ester

There total 1 articles about 2,4-Dimethoxy-benzoic acid (1R,3R,4R,5S,11S)-3-(2-amino-6-chloro-purin-9-yl)-7,7,9,9-tetraisopropyl-6,8,10-trioxa-2-thia-7,9-disila-tricyclo[9.3.0.0^1,5]tetradec-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

2,4-Dimethoxy-benzoic acid (1R,2R,4R,5S,11S)-7,7,9,9-tetraisopropyl-2-oxo-6,8,10-trioxa-2λ4-thia-7,9-disila-tricyclo[9.3.0.01,5]tetradec-4-yl ester (862080-84-0) + 2-Amino-6-chloropurin (10310-21-1) → (1R,2S,5S,11S)-7,7,9,9-Tetraisopropyl-6,8,10-trioxa-2-thia-7,9-disila-tricyclo[9.3.0.01,5]tetradec-3-ene 2-oxide + 2,4-Dimethoxy-benzoic acid (1R,3R,4R,5S,11S)-3-(2-amino-6-chloro-purin-9-yl)-7,7,9,9-tetraisopropyl-6,8,10-trioxa-2-thia-7,9-disila-tricyclo[9.3.0.01,5]tetradec-4-yl ester (862081-05-8) + 2,4-Dimethoxy-benzoic acid (1R,3R,4R,5S,11S)-3-(2-amino-6-chloro-purin-7-yl)-7,7,9,9-tetraisopropyl-6,8,10-trioxa-2-thia-7,9-disila-tricyclo[9.3.0.01,5]tetradec-4-yl ester

Guidance literature:

2-Amino-6-chloropurin; With trimethylsilyl trifluoromethanesulfonate; triethylamine; In 1,2-dichloro-ethane; acetonitrile; at 20 ℃; for 1h;

2,4-Dimethoxy-benzoic acid (1R,2R,4R,5S,11S)-7,7,9,9-tetraisopropyl-2-oxo-6,8,10-trioxa-2λ⁴-thia-7,9-disila-tricyclo[9.3.0.0^1,5]tetradec-4-yl ester; With triethylamine; In 1,2-dichloro-ethane; acetonitrile; for 24h; Heating;

DOI:10.1021/jo0506985

Reference yield:

2,4-Dimethoxy-benzoic acid (1R,3R,4R,5S,11S)-3-(2-amino-6-chloro-purin-9-yl)-7,7,9,9-tetraisopropyl-6,8,10-trioxa-2-thia-7,9-disila-tricyclo[9.3.0.01,5]tetradec-4-yl ester (862081-05-8) → 2,4-Dimethoxy-benzoic acid (2R,3R,4S,5R,6S)-2-(2-amino-6-chloro-purin-9-yl)-4,6-dihydroxy-1-thia-spiro[4.4]non-3-yl ester

Guidance literature:

With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 20 ℃; for 0.166667h;

DOI:10.1021/jo0506985

upstream raw materials:

2,4-Dimethoxy-benzoic acid (1R,2R,4R,5S,11S)-7,7,9,9-tetraisopropyl-2-oxo-6,8,10-trioxa-2λ⁴-thia-7,9-disila-tricyclo[9.3.0.0^1,5]tetradec-4-yl ester

2-Amino-6-chloropurin

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