1-ethoxymethyl-5-methylthio-2-phenylthioimidazole-4-carboxyli acid

Base Information

Chemical Name:1-ethoxymethyl-5-methylthio-2-phenylthioimidazole-4-carboxyli acid
CAS No.:81356-75-4
Molecular Formula:C₁₄H₁₆N₂O₃S₂
Molecular Weight:324.425
Hs Code.:

Synonyms:1-ethoxymethyl-5-methylthio-2-phenylthioimidazole-4-carboxyli acid

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Chemical Property of 1-ethoxymethyl-5-methylthio-2-phenylthioimidazole-4-carboxyli acid

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Technology Process of 1-ethoxymethyl-5-methylthio-2-phenylthioimidazole-4-carboxyli acid

There total 3 articles about 1-ethoxymethyl-5-methylthio-2-phenylthioimidazole-4-carboxyli acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 124-38-9,18923-20-1
carbon dioxide

: 81356-73-2
4-bromo-1-ethoxymethyl-5-methylthio-2-phenylthioimidazole

: 81356-75-4
1-ethoxymethyl-5-methylthio-2-phenylthioimidazole-4-carboxyli acid

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; 1.) -70 deg C, 1 h, 2.) room temperature;

Reference yield:

: 81356-68-5
1-ethoxymethyl-5-methylthio-2-phenylthioimidazole

: 81356-75-4
1-ethoxymethyl-5-methylthio-2-phenylthioimidazole-4-carboxyli acid

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / bromination

2: 74 percent / nBuLi / diethyl ether / -70 °C

With n-butyllithium; In diethyl ether;
DOI:10.1039/c39810001095

Reference yield:

: 67319-06-6
1-ethoxymethyl-5-lithio-2-phenylthioimidazole

: 81356-75-4
1-ethoxymethyl-5-methylthio-2-phenylthioimidazole-4-carboxyli acid

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / nBuLi / tetrahydrofuran / -78 °C

2: 92 percent / bromination

3: 74 percent / nBuLi / diethyl ether / -70 °C

With n-butyllithium; In tetrahydrofuran; diethyl ether;
DOI:10.1039/c39810001095