phenylmercury trichloroacetate

Base Information

Chemical Name:phenylmercury trichloroacetate
CAS No.:14076-29-0
Molecular Formula:C₈H₅Cl₃HgO₂
Molecular Weight:440.075
Hs Code.:

Synonyms:phenylmercury trichloroacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenylmercury trichloroacetate

Chemical Property:

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Technology Process of phenylmercury trichloroacetate

There total 3 articles about phenylmercury trichloroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 12653-71-3
mercury(II) oxide

: 76-03-9
trichloroacetic acid

: 14076-29-0
phenylmercury trichloroacetate

Guidance literature:: With benzene; In benzene; (N2), heated at 60-70°C for 4 h; filtered hot, solvent removed under reduced pressure, concentrate kept in a deep freeze, recrystd. from CH2Cl2, elem. anal.;

Reference yield: 85.0%

: 587-85-9,1337-09-3
diphenylmercury(II)

: 76-03-9
trichloroacetic acid

: 14076-29-0
C₆H₅Hg⁽¹⁺⁾*CCl₃COO^(1-) = C₆H₅HgOCOCCl₃

Guidance literature:: In tetrahydrofuran; byproducts: C6H6; stirring (3-4 h, 0°C); pptn. (petroleum ether), concn. (vac.), recrystn. (CH2Cl2/hexane); elem.anal.;

Reference yield:

: 12653-71-3
mercury(II) oxide

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 76-03-9
trichloroacetic acid

: 14076-29-0
phenylmercury trichloroacetate

Guidance literature:: In benzene; byproducts: H2O; HgO added with stirring to Cl3CCOOH in benzene soln., left for 12h; filtered, partially evapd. without heating in vac., pptn. with ethanol, filtered, washed twice with ethanol, purified by evapn. of acetone soln. without heating in vac., filtered, crystals washed with acetone;