5,6-dihydro-1,2-bis(methoxycarbonyl)-3-phenyl-4H-benzopyrrolo<2,1,5-cd>indolizine

Base Information

Chemical Name:5,6-dihydro-1,2-bis(methoxycarbonyl)-3-phenyl-4H-benzopyrrolo<2,1,5-cd>indolizine
CAS No.:99682-37-8
Molecular Formula:C₂₃H₁₉NO₄
Molecular Weight:373.408
Hs Code.:

5,6-dihydro-1,2-bis(methoxycarbonyl)-3-phenyl-4H-benzo<hi>pyrrolo<2,1,5-cd>indolizine

Synonyms:5,6-dihydro-1,2-bis(methoxycarbonyl)-3-phenyl-4H-benzopyrrolo<2,1,5-cd>indolizine

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Chemical Property of 5,6-dihydro-1,2-bis(methoxycarbonyl)-3-phenyl-4H-benzopyrrolo<2,1,5-cd>indolizine

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Technology Process of 5,6-dihydro-1,2-bis(methoxycarbonyl)-3-phenyl-4H-benzopyrrolo<2,1,5-cd>indolizine

There total 4 articles about 5,6-dihydro-1,2-bis(methoxycarbonyl)-3-phenyl-4H-benzopyrrolo<2,1,5-cd>indolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 120161-18-4
1-phenyl-8,9-dihydro-7H-pyrrolo<3,2,1-ij>quinoline

: 762-42-5
dimethyl acetylenedicarboxylate

: 99682-37-8
5,6-dihydro-1,2-bis(methoxycarbonyl)-3-phenyl-4H-benzopyrrolo<2,1,5-cd>indolizine

Guidance literature:: palladium on activated charcoal; In toluene; for 50h; Heating;
DOI:10.1002/jhet.5570220425

Reference yield:

: 10500-57-9
5,6,7,8-tetrahydroquinoline

: 99682-37-8
5,6-dihydro-1,2-bis(methoxycarbonyl)-3-phenyl-4H-benzopyrrolo<2,1,5-cd>indolizine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / acetone / 1) 2 h, reflux; 2) room temp., overnight

2: 88 percent / NaHCO₃ / ethanol / Heating; overnight

3: 58 percent / Pd/C / toluene / 50 h / Heating

With sodium hydrogencarbonate; palladium on activated charcoal; In ethanol; acetone; toluene;
DOI:10.1002/jhet.5570220425

Reference yield:

: 102408-79-7
5,6,7,8-tetrahydro-1-phenacylquinolinium bromide

: 99682-37-8
5,6-dihydro-1,2-bis(methoxycarbonyl)-3-phenyl-4H-benzopyrrolo<2,1,5-cd>indolizine

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / NaHCO₃ / ethanol / Heating; overnight

2: 58 percent / Pd/C / toluene / 50 h / Heating

With sodium hydrogencarbonate; palladium on activated charcoal; In ethanol; toluene;
DOI:10.1002/jhet.5570220425