3-benzoyl-2,2-dimethyl-3,4,5,6,7,8-hexahydro-2H-cyclohepta[d][1,3]thiazole

Base Information

Chemical Name:3-benzoyl-2,2-dimethyl-3,4,5,6,7,8-hexahydro-2H-cyclohepta[d][1,3]thiazole
CAS No.:1571129-23-1
Molecular Formula:C₁₇H₂₁NOS
Molecular Weight:287.426
Hs Code.:

Synonyms:3-benzoyl-2,2-dimethyl-3,4,5,6,7,8-hexahydro-2H-cyclohepta[d][1,3]thiazole

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Chemical Property of 3-benzoyl-2,2-dimethyl-3,4,5,6,7,8-hexahydro-2H-cyclohepta[d][1,3]thiazole

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Technology Process of 3-benzoyl-2,2-dimethyl-3,4,5,6,7,8-hexahydro-2H-cyclohepta[d][1,3]thiazole

There total 5 articles about 3-benzoyl-2,2-dimethyl-3,4,5,6,7,8-hexahydro-2H-cyclohepta[d][1,3]thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1571129-41-3
(RS)-3-benzoyl-2,2-dimethyl-4-methoxy-1-thia-3-azaspiro[4.5]decane

: 100-66-3
methoxybenzene

: (3aS*,8aS*)-3-benzoyl-8a-(4-methoxyphenyl)-2,2-dimethyloctahydro-2H-cyclohepta[d][1,3]thiazole

: 1571129-23-1
3-benzoyl-2,2-dimethyl-3,4,5,6,7,8-hexahydro-2H-cyclohepta[d][1,3]thiazole

Guidance literature:: (RS)-3-benzoyl-2,2-dimethyl-4-methoxy-1-thia-3-azaspiro[4.5]decane; With aluminum (III) chloride; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere; Schlenk technique;

methoxybenzene; In dichloromethane; at 0 - 20 ℃; for 120h; diastereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1002/hc.21131

Reference yield: 35.0%

: 1571129-41-3
(RS)-3-benzoyl-2,2-dimethyl-4-methoxy-1-thia-3-azaspiro[4.5]decane

: 1571129-23-1
3-benzoyl-2,2-dimethyl-3,4,5,6,7,8-hexahydro-2H-cyclohepta[d][1,3]thiazole

Guidance literature:: With aluminum (III) chloride; In dichloromethane; at 0 - 20 ℃; for 120h; Inert atmosphere; Schlenk technique;
DOI:10.1002/hc.21131

Reference yield:

: 53627-10-4
1-chlorocyclohexane-1-carbaldehyde

: 1571129-23-1
3-benzoyl-2,2-dimethyl-3,4,5,6,7,8-hexahydro-2H-cyclohepta[d][1,3]thiazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogensulfide; ammonium hydroxide / dichloromethane

2.1: dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2.2: 0 - 20 °C / Inert atmosphere; Schlenk technique

3.1: aluminum (III) chloride / dichloromethane / 120 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

With aluminum (III) chloride; ammonium hydroxide; sodium hydrogensulfide; In dichloromethane; 1.1: |Asinger Thiazoline Synthesis;
DOI:10.1002/hc.21131