N,N-bis-(2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexylidene)ethylamino]ethyl)maleamic acid

Base Information

Chemical Name:N,N-bis-(2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexylidene)ethylamino]ethyl)maleamic acid
CAS No.:1350564-34-9
Molecular Formula:C₂₈H₃₉N₃O₇
Molecular Weight:529.634
Hs Code.:

Synonyms:N,N-bis-(2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexylidene)ethylamino]ethyl)maleamic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-bis-(2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexylidene)ethylamino]ethyl)maleamic acid

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Technology Process of N,N-bis-(2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexylidene)ethylamino]ethyl)maleamic acid

There total 2 articles about N,N-bis-(2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexylidene)ethylamino]ethyl)maleamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-31-6
maleic anhydride

: 296269-80-2
N,N-bis(1-(4,4-dimethyl-2,6-dioxocyclohexyliden)ethyl)diethylenetriamine

: 1350564-34-9
N,N-bis-(2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexylidene)ethylamino]ethyl)maleamic acid

Guidance literature:: In dichloromethane; for 8h;
DOI:10.1039/c1cc15805h

Reference yield:

: 94142-97-9
2-(1-hydroxyethylidene)-5,5-dimethylcyclohexane-1,3-dione

: 1350564-34-9
N,N-bis-(2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexylidene)ethylamino]ethyl)maleamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 6 h

2: dichloromethane / 8 h

In dichloromethane;
DOI:10.1039/c1cc15805h

Reference yield:

: 1350564-34-9
N,N-bis-(2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexylidene)ethylamino]ethyl)maleamic acid

: C₇₄H₁₀₃N₁₄O₁₆PolS₃

: C₁₀₂H₁₄₀N₁₇O₂₂PolS₃

Guidance literature:: With benzotriazol-1-ol; diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 60 ℃; for 0.333333h; Microwave irradiation; solid phase reaction;
DOI:10.1039/c1cc15805h