furan-2-yl[2-methoxy-5-(4-methoxyphenyl)furan-3-yl]diphenylphosphonium tetrafluoroborate

Base Information

• Chemical Name: furan-2-yl[2-methoxy-5-(4-methoxyphenyl)furan-3-yl]diphenylphosphonium tetrafluoroborate
• CAS No.: 1448326-08-6
• Molecular Formula: BF₄*C₂₈H₂₄O₄P
• Molecular Weight: 542.275

Synonyms:furan-2-yl[2-methoxy-5-(4-methoxyphenyl)furan-3-yl]diphenylphosphonium tetrafluoroborate

Chemical Property of furan-2-yl[2-methoxy-5-(4-methoxyphenyl)furan-3-yl]diphenylphosphonium tetrafluoroborate

Chemical Property:

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Technology Process of furan-2-yl[2-methoxy-5-(4-methoxyphenyl)furan-3-yl]diphenylphosphonium tetrafluoroborate

There total 2 articles about furan-2-yl[2-methoxy-5-(4-methoxyphenyl)furan-3-yl]diphenylphosphonium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

[furan-2-yl(diphenyl)phosphonio](methoxycarbonyl) (1448325-79-8) + 4-methoxyphenylacetylen (768-60-5) → furan-2-yl[2-methoxy-5-(4-methoxyphenyl)furan-3-yl]diphenylphosphonium tetrafluoroborate (1448326-08-6) + methyl 7-(4-methoxyphenyl)-4,4-diphenyl-4λ5-phosphinino[3,2-b]furan-5-carboxylate + methyl 2-[6-(methoxycarbonyl)-4-(4-methoxyphenyl)-2-(2-oxoethyl)-1,1-diphenyl-1λ5-phosphinin-3-yl]-7-(4-methoxyphenyl)-4,4-diphenyl-4λ5-phosphinino[3,2-b]furan-5-carboxylate + (furan-2-yl)(2-methoxy-2-oxoethyl)diphenylphosphonium tetrafluoroborate

Guidance literature:

In dichloromethane; UV-irradiation; Inert atmosphere;

DOI:10.1002/ejoc.201500876

Reference yield: 15.0%

[furan-2-yl(diphenyl)phosphonio](methoxycarbonyl) (1448325-79-8) + 4-methoxyphenylacetylen (768-60-5) → furan-2-yl[2-methoxy-5-(4-methoxyphenyl)furan-3-yl]diphenylphosphonium tetrafluoroborate (1448326-08-6) + methyl 4-(4-methoxyphenyl)-7,7-diphenyl-7λ5-phosphinino[2,3-b]furan-6-carboxylate (1448326-09-7)

Guidance literature:

In dichloromethane;

DOI:10.1016/j.tet.2013.06.066

upstream raw materials:

[furan-2-yl(diphenyl)phosphonio](methoxycarbonyl)

4-methoxyphenylacetylen

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