C₄₅H₆₁FN₈O₅

Base Information

Chemical Name:C₄₅H₆₁FN₈O₅
CAS No.:1009092-89-0
Molecular Formula:C₄₅H₆₁FN₈O₅
Molecular Weight:813.028
Hs Code.:

C<sub>45</sub>H<sub>61</sub>FN<sub>8</sub>O<sub>5</sub>

Synonyms:C₄₅H₆₁FN₈O₅

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Chemical Property of C₄₅H₆₁FN₈O₅

Chemical Property:

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Technology Process of C₄₅H₆₁FN₈O₅

There total 13 articles about C₄₅H₆₁FN₈O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1009092-88-9
C₃₄H₄₅FN₆O₆

: 29802-26-4
N-[(2S)-2-amino-3-phenylpropyl]-N,N-dimethylamine

: 1009092-89-0
C₄₅H₆₁FN₈O₅

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In dichloromethane; for 2h;

Reference yield:

: 3-bromo-6-fluoro-2-hydroxybenzaldehyde

: 1009092-89-0
C₄₅H₆₁FN₈O₅

Guidance literature:: Multi-step reaction with 11 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 40 °C

2.1: hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 0.08 h / 20 °C

3.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 3 h / pH 2

4.1: calcium chloride / diethyl ether / 3 h / 20 °C

5.1: titanium(IV) isopropylate / tetrahydrofuran / 0.17 h / 140 °C / Microwave irradiation

6.1: hydrogenchloride / tetrahydrofuran; water / 1.5 h / 20 °C

6.2: pH 7

7.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / 0 °C

8.1: sodium azide / dichloromethane; N,N-dimethyl-formamide / 20 °C

9.1: diisobutylaluminium hydride / tetrahydrofuran; dichloromethane / 2.5 h / 0 - 20 °C

9.2: 0.5 h / 20 °C

9.3: 2 h

10.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 3 h / 70 °C

11.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 2 h

With titanium(IV) isopropylate; hydrogenchloride; sodium azide; hydroxylamine hydrochloride; methyl orange; potassium acetate; diisobutylaluminium hydride; sodium cyanoborohydride; potassium carbonate; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; calcium chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 473416-74-9
3-bromo-6-fluoro-2-methoxybenzaldehyde

: 1009092-89-0
C₄₅H₆₁FN₈O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 0.08 h / 20 °C

2.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 3 h / pH 2

3.1: calcium chloride / diethyl ether / 3 h / 20 °C

4.1: titanium(IV) isopropylate / tetrahydrofuran / 0.17 h / 140 °C / Microwave irradiation

5.1: hydrogenchloride / tetrahydrofuran; water / 1.5 h / 20 °C

5.2: pH 7

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / 0 °C

7.1: sodium azide / dichloromethane; N,N-dimethyl-formamide / 20 °C

8.1: diisobutylaluminium hydride / tetrahydrofuran; dichloromethane / 2.5 h / 0 - 20 °C

8.2: 0.5 h / 20 °C

8.3: 2 h

9.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 3 h / 70 °C

10.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 2 h

With titanium(IV) isopropylate; hydrogenchloride; sodium azide; hydroxylamine hydrochloride; methyl orange; potassium acetate; diisobutylaluminium hydride; sodium cyanoborohydride; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; calcium chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;