mesityl(fluorenyl)germane

Base Information

Chemical Name:mesityl(fluorenyl)germane
CAS No.:154707-06-9
Molecular Formula:C₂₂H₂₂Ge
Molecular Weight:359.007
Hs Code.:

Synonyms:mesityl(fluorenyl)germane

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Chemical Property of mesityl(fluorenyl)germane

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Technology Process of mesityl(fluorenyl)germane

There total 2 articles about mesityl(fluorenyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 134691-77-3
mesitylfluorenyldichlorogermane

: 154707-06-9
mesityl(fluorenyl)germane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; high-vac. line technique, O2-free; slow addn. of soln. of Ge-compd. in Et2O to soln. of LiAlH4 in Et2O at 0°C, stirring for 0.5 h; mixture is hydrolyzed, organic layer is extracted with Et2O, dryed over Na2SO4 and cooled;
DOI:10.1016/0022-328X(94)88005-0

Reference yield:

: 154707-07-0
mesityl(fluorenyl)chlorogermane

: (C₆H₂(CH₃)3)GeH(CHC₁₂H₈)GeH(C₆H₂(CH₃)3)(CHC₁₂H₈)

: 154707-06-9
mesityl(fluorenyl)germane

Guidance literature:: With amalgamated magnesium; In tetrahydrofuran; high-vac. line technique, O2-free; soln. of Ge-compd. in THF is added to Mg-amalgam, refluxing for 1 h; hydrolyzing, drying over Na2SO4, product identification by NMR-spectroscopy, mixture of 2 diastereoisomers is formed in 20% yield which are separated by fractional crystn. from Et2O, main product is the mesityl(fluorenyl)germane;
DOI:10.1016/0022-328X(94)88005-0