mesitylfluorenyldichlorogermane

Base Information

Chemical Name:mesitylfluorenyldichlorogermane
CAS No.:134691-77-3
Molecular Formula:C₂₂H₂₀Cl₂Ge
Molecular Weight:427.897
Hs Code.:

Synonyms:mesitylfluorenyldichlorogermane

Suppliers and Price of mesitylfluorenyldichlorogermane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of mesitylfluorenyldichlorogermane

Chemical Property:

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Technology Process of mesitylfluorenyldichlorogermane

There total 2 articles about mesitylfluorenyldichlorogermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 134691-74-0
mesitylfluorenyldimethoxygermane

: 134691-77-3
mesitylfluorenyldichlorogermane

Guidance literature:: With hydrogenchloride; In diethyl ether; byproducts: CH3OH, fluorene; (N2 or Ar); addn. of compounds at -78°C; warmed to room temp.; evapn. in vacuo; fractional crystn. in pentane; filtration;

Reference yield:

: 114806-82-5
(2,4,6-trimethylphenyl)trichlorogermane

: 881-04-9
9H-fluoren-9-yllithium

: 134691-77-3
mesitylfluorenyldichlorogermane

: 154707-16-1
mesityl(difluorenyl)chlorogermane

Guidance literature:: In diethyl ether; high-vac. line technique, O2-free; addn. of fluorenyllithium (from n-BuLi and fluorene in hexane) to a soln. of Ge-compd. in Et2O, stirring for 1 h at room temp.; filtn., recrystn. from pentane, products identified by NMR-spectroscopy;
DOI:10.1016/0022-328X(94)88005-0

Reference yield: 91.0%

: 134691-77-3
mesitylfluorenyldichlorogermane

: 154707-06-9
mesityl(fluorenyl)germane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; high-vac. line technique, O2-free; slow addn. of soln. of Ge-compd. in Et2O to soln. of LiAlH4 in Et2O at 0°C, stirring for 0.5 h; mixture is hydrolyzed, organic layer is extracted with Et2O, dryed over Na2SO4 and cooled;
DOI:10.1016/0022-328X(94)88005-0