3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid dimethyl ester

Base Information

• Chemical Name: 3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid dimethyl ester
• CAS No.: 84801-91-2
• Molecular Formula: C₂₃H₁₆N₂O₇
• Molecular Weight: 432.389

Synonyms:3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid dimethyl ester

Chemical Property of 3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid dimethyl ester

Chemical Property:

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Technology Process of 3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid dimethyl ester

There total 2 articles about 3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

C17H13N2O3(1+)*I(1-) (6277-71-0) + dimethyl acetylenedicarboxylate (762-42-5) → 3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid dimethyl ester (84801-91-2)

Guidance literature:

With iodine; In dimethyl sulfoxide; at 20 ℃; for 2h;

DOI:10.1007/s00706-013-1120-6

Reference yield: 58.0%

2-(2-(4-nitrophenyl)-2-oxoethyl)isoquinolin-2-ium bromide (39954-59-1) + dimethyl acetylenedicarboxylate (762-42-5) → 3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid dimethyl ester (84801-91-2)

Guidance literature:

With triethylamine; In benzene; 1.) 1 h, 2.) reflux, 6 h;

DOI:10.1021/je00032a044

upstream raw materials:

2-(2-(4-nitrophenyl)-2-oxoethyl)isoquinolin-2-ium bromide

dimethyl acetylenedicarboxylate

C₁₇H₁₃N₂O₃⁽¹⁺⁾*I^(1-)

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