chloro(phenyliodophosphine)(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) iodide

Base Information

Chemical Name:chloro(phenyliodophosphine)(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) iodide
CAS No.:102808-43-5
Molecular Formula:C₄₉H₄₃ClIOOsP₄*I
Molecular Weight:1251.24
Hs Code.:

Synonyms:chloro(phenyliodophosphine)(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) iodide

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Chemical Property of chloro(phenyliodophosphine)(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) iodide

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Technology Process of chloro(phenyliodophosphine)(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) iodide

There total 2 articles about chloro(phenyliodophosphine)(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 102781-82-8
(phenylphosphido)chloro(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II)

: 102808-43-5
chloro(phenyliodophosphine)(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) iodide

Guidance literature:: With I₂; In benzene; N2-atmosphere; dropwise addn. of benzene soln. of I2 to suspn. of Os-complex in benzene; 30 min, 25. degree.C;; cooling in ice bath and addn. of hexane; filtration; recrystn. from CH2Cl2/EtOH; elem. anal.;

Reference yield:

: 102747-27-3
chlorobis(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) perchlorate

: 102808-43-5
chloro(phenyliodophosphine)(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / methanol

2: I₂ / benzene

With 1,8-diazabicyclo[5.4.0]undec-7-ene; I₂; In methanol; benzene;