chlorobis(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) perchlorate

Base Information

Chemical Name:chlorobis(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) perchlorate
CAS No.:102747-27-3
Molecular Formula:C₄₉H₄₄ClOOsP₄*ClO₄
Molecular Weight:1097.89
Hs Code.:

Synonyms:chlorobis(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) perchlorate

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Chemical Property of chlorobis(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) perchlorate

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Technology Process of chlorobis(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) perchlorate

There total 1 articles about chlorobis(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 102849-33-2
chloro(phenylphosphine)(acetonitrile)carbonylbis(triphenylphosphine)osmium(II) perchlorate

: 638-21-1
phenylphosphane

: 102747-27-3
chlorobis(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) perchlorate

Guidance literature:: In chloroform; benzene; inert atmosphere; addn. of PH2Ph in C6H6 to soln. of Os-complex in CHCl3; refluxing at 62°C for 24 h;; cooling; removal of volatiles under vac.; recrystn. from CH2Cl2/EtOH; elem. anal.;

Reference yield: 95.0%

: 102747-27-3
chlorobis(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) perchlorate

: 102781-82-8
(phenylphosphido)chloro(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II)

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In benzene; N2-atmosphere; addn. of DBU to suspn. of Os-complex; stirring for 45 min;; cooling; addn. of dried MeOH; filtration after 5 min; washing (MeOH, EtOH, hexane);;

Reference yield:

: 102747-27-3
chlorobis(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) perchlorate

: 102808-43-5
chloro(phenyliodophosphine)(phenylphosphine)carbonylbis(triphenylphosphine)osmium(II) iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / methanol

2: I₂ / benzene

With 1,8-diazabicyclo[5.4.0]undec-7-ene; I₂; In methanol; benzene;