(3S,4S)-1-(2-benzyloxyethyl)-3,4-bis(trifluoromethanesulfonyloxy)pyrrolidine

Base Information

Chemical Name:(3S,4S)-1-(2-benzyloxyethyl)-3,4-bis(trifluoromethanesulfonyloxy)pyrrolidine
CAS No.:871822-39-8
Molecular Formula:C₁₅H₁₇F₆NO₇S₂
Molecular Weight:501.425
Hs Code.:

Synonyms:(3S,4S)-1-(2-benzyloxyethyl)-3,4-bis(trifluoromethanesulfonyloxy)pyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S)-1-(2-benzyloxyethyl)-3,4-bis(trifluoromethanesulfonyloxy)pyrrolidine

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Technology Process of (3S,4S)-1-(2-benzyloxyethyl)-3,4-bis(trifluoromethanesulfonyloxy)pyrrolidine

There total 1 articles about (3S,4S)-1-(2-benzyloxyethyl)-3,4-bis(trifluoromethanesulfonyloxy)pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: (3S,4S)-1-(2-benzyloxyethyl)pyrrolidine-3,4-diol

: 358-23-6
trifluoromethylsulfonic anhydride

: 871822-39-8
(3S,4S)-1-(2-benzyloxyethyl)-3,4-bis(trifluoromethanesulfonyloxy)pyrrolidine

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1021/jo0513414

Reference yield:

: 871822-39-8
(3S,4S)-1-(2-benzyloxyethyl)-3,4-bis(trifluoromethanesulfonyloxy)pyrrolidine

: 871822-43-4
(3R,4R)-1-(2-hydroxyethyl)-3,4-difluoropyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 20 h / 20 °C

2: 66 percent / boron trichloride/dimethyl sulfide complex / CH₂Cl₂ / 4 h / 20 °C

With dimethylsulfide; tetrabutyl ammonium fluoride; boron trichloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo0513414