5-(acetoxy(p-tolyl)amino)-5-oxo-1-(trimethylsilyl)pentan-2-yl O-ethylcarbonodithioate

Base Information

Chemical Name:5-(acetoxy(p-tolyl)amino)-5-oxo-1-(trimethylsilyl)pentan-2-yl O-ethylcarbonodithioate
CAS No.:1403889-64-4
Molecular Formula:C₂₀H₃₁NO₄S₂Si
Molecular Weight:441.688
Hs Code.:

Synonyms:5-(acetoxy(p-tolyl)amino)-5-oxo-1-(trimethylsilyl)pentan-2-yl O-ethylcarbonodithioate

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Chemical Property of 5-(acetoxy(p-tolyl)amino)-5-oxo-1-(trimethylsilyl)pentan-2-yl O-ethylcarbonodithioate

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Technology Process of 5-(acetoxy(p-tolyl)amino)-5-oxo-1-(trimethylsilyl)pentan-2-yl O-ethylcarbonodithioate

There total 5 articles about 5-(acetoxy(p-tolyl)amino)-5-oxo-1-(trimethylsilyl)pentan-2-yl O-ethylcarbonodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1403889-59-7
S-2-(acetoxy(p-tolyl)amino)-2-oxoethyl O-ethyl carbonodithioate

: 762-72-1
allyl-trimethyl-silane

: 1403889-64-4
5-(acetoxy(p-tolyl)amino)-5-oxo-1-(trimethylsilyl)pentan-2-yl O-ethylcarbonodithioate

Guidance literature:: With dilauryl peroxide; In ethyl acetate; for 5h; Reflux; Inert atmosphere;
DOI:10.1021/ol3026044

Reference yield:

: 623-10-9
N-(4-methylphenyl)hydroxylamine

: 1403889-64-4
5-(acetoxy(p-tolyl)amino)-5-oxo-1-(trimethylsilyl)pentan-2-yl O-ethylcarbonodithioate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / diethyl ether; water / -5 °C / Cooling with ice; Inert atmosphere

2: acetic anhydride / 20 °C / Inert atmosphere

3: acetone / 6 h / 0 °C / Inert atmosphere

4: dilauryl peroxide / ethyl acetate / 5 h / Reflux; Inert atmosphere

With dilauryl peroxide; acetic anhydride; sodium hydrogencarbonate; In diethyl ether; water; ethyl acetate; acetone;
DOI:10.1021/ol3026044

Reference yield:

: 1403889-48-4
N-(4-methylphenyl)-2-chloro-N-hydroxyacetamide

: 1403889-64-4
5-(acetoxy(p-tolyl)amino)-5-oxo-1-(trimethylsilyl)pentan-2-yl O-ethylcarbonodithioate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic anhydride / 20 °C / Inert atmosphere

2: acetone / 6 h / 0 °C / Inert atmosphere

3: dilauryl peroxide / ethyl acetate / 5 h / Reflux; Inert atmosphere

With dilauryl peroxide; acetic anhydride; In ethyl acetate; acetone;
DOI:10.1021/ol3026044