C₂₈H₃₃NO₄S

Base Information

Chemical Name:C₂₈H₃₃NO₄S
CAS No.:1375101-99-7
Molecular Formula:C₂₈H₃₃NO₄S
Molecular Weight:479.64
Hs Code.:

C<sub>28</sub>H<sub>33</sub>NO<sub>4</sub>S

Synonyms:C₂₈H₃₃NO₄S

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Chemical Property of C₂₈H₃₃NO₄S

Chemical Property:

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Technology Process of C₂₈H₃₃NO₄S

There total 3 articles about C₂₈H₃₃NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1290631-83-2
(1R,5S)-tert-butyl-7-[N-benzyl-4-methylphenylsulfonamido]-6-cyclohexyl-2-oxobicyclo[3.2.0]hept-6-ene-1-carboxylate

: 1375101-99-7
C₂₈H₃₃NO₄S

: 1375101-98-6
N-benzyl-N-[(1S,4S,5S)-7-cyclohexyl-4-hydroxy-5-(hydroxymethyl)bicyclo[3.2.0]hept-6-en-6-yl]-4-methylbenzenesulfonamide

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃; for 2.5h; Inert atmosphere;
DOI:10.1055/s-0031-1289679

Reference yield:

: 1116153-61-7
N-benzyl-N-(cyclohexylethynyl)-4-methylbenzenesulfonamide

: 1375101-99-7
C₂₈H₃₃NO₄S

: 1375101-98-6
N-benzyl-N-[(1S,4S,5S)-7-cyclohexyl-4-hydroxy-5-(hydroxymethyl)bicyclo[3.2.0]hept-6-en-6-yl]-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: RuCl2(κ4-N,N'-bis[o-(diphenylphosphino)benzylidene]-(1S,2S)-diiminocyclohexane); triethyloxonium hexaflourophosphate / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

1.2: 24 h / 55 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / diethyl ether / 2.5 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; RuCl2(κ4-N,N'-bis[o-(diphenylphosphino)benzylidene]-(1S,2S)-diiminocyclohexane); triethyloxonium hexaflourophosphate; In diethyl ether; dichloromethane; 1.1: Ficini reaction / 1.2: Ficini reaction;
DOI:10.1055/s-0031-1289679

Reference yield:

: tert‐butyl 5‐oxocyclopent‐1‐ene‐1‐carboxylate

: 1375101-99-7
C₂₈H₃₃NO₄S

: 1375101-98-6
N-benzyl-N-[(1S,4S,5S)-7-cyclohexyl-4-hydroxy-5-(hydroxymethyl)bicyclo[3.2.0]hept-6-en-6-yl]-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: RuCl2(κ4-N,N'-bis[o-(diphenylphosphino)benzylidene]-(1S,2S)-diiminocyclohexane); triethyloxonium hexaflourophosphate / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

1.2: 24 h / 55 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / diethyl ether / 2.5 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; RuCl2(κ4-N,N'-bis[o-(diphenylphosphino)benzylidene]-(1S,2S)-diiminocyclohexane); triethyloxonium hexaflourophosphate; In diethyl ether; dichloromethane; 1.1: Ficini reaction / 1.2: Ficini reaction;
DOI:10.1055/s-0031-1289679