N-[2-(5-methoxy-2-nitrophenyl)ethyl]-1-(phenylmethyl)-4-piperidineamine

Base Information

Chemical Name:N-[2-(5-methoxy-2-nitrophenyl)ethyl]-1-(phenylmethyl)-4-piperidineamine
CAS No.:337910-18-6
Molecular Formula:C₂₁H₂₇N₃O₃
Molecular Weight:369.464
Hs Code.:

Synonyms:N-[2-(5-methoxy-2-nitrophenyl)ethyl]-1-(phenylmethyl)-4-piperidineamine

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Chemical Property of N-[2-(5-methoxy-2-nitrophenyl)ethyl]-1-(phenylmethyl)-4-piperidineamine

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Technology Process of N-[2-(5-methoxy-2-nitrophenyl)ethyl]-1-(phenylmethyl)-4-piperidineamine

There total 5 articles about N-[2-(5-methoxy-2-nitrophenyl)ethyl]-1-(phenylmethyl)-4-piperidineamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3612-20-2
1-phenylmethyl-4-piperidone

: 180149-25-1
2-(5-methoxy-2-nitrophenyl)-ethylamine

: 337910-18-6
N-[2-(5-methoxy-2-nitrophenyl)ethyl]-1-(phenylmethyl)-4-piperidineamine

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

Reference yield: 100.0%

: 4783-65-7
N-benzyl-2-piperidinone

: 180149-25-1
2-(5-methoxy-2-nitrophenyl)-ethylamine

: 337910-18-6
N-[2-(5-methoxy-2-nitrophenyl)ethyl]-1-(phenylmethyl)-4-piperidineamine

Guidance literature:: N-benzyl-2-piperidinone; 2-(5-methoxy-2-nitrophenyl)-ethylamine; With acetic acid; In dichloromethane; at 0 ℃; Inert atmosphere;

With sodium tris(acetoxy)borohydride; In dichloromethane; for 0.333333h;

Reference yield: 43.0%

: 337910-19-7
5-methoxy-2-nitro-N-[1-(phenylmethyl)-4-piperidinyl]-benzeneacetamide

: 337910-18-6
N-[2-(5-methoxy-2-nitrophenyl)ethyl]-1-(phenylmethyl)-4-piperidineamine

Guidance literature:: 5-methoxy-2-nitro-N-[1-(phenylmethyl)-4-piperidinyl]-benzeneacetamide; With chloro-trimethyl-silane; In tetrahydrofuran; at 20 ℃; for 1h;

With lithium borohydride; In tetrahydrofuran; at 20 ℃; for 4.5h; Heating / reflux;

With hydrogenchloride; ammonia; water; more than 3 stages;