1,3,4,6-Tetrakis(acetoxymethyl)tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione

Base Information

• Chemical Name: 1,3,4,6-Tetrakis(acetoxymethyl)tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione
• CAS No.: 154230-91-8
• Molecular Formula: C₂₈H₃₀N₄O₁₀
• Molecular Weight: 582.567

Synonyms:1,3,4,6-Tetrakis(acetoxymethyl)tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione

Chemical Property of 1,3,4,6-Tetrakis(acetoxymethyl)tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione

Chemical Property:

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Technology Process of 1,3,4,6-Tetrakis(acetoxymethyl)tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione

There total 3 articles about 1,3,4,6-Tetrakis(acetoxymethyl)tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

acetic anhydride (108-24-7) + 1,6:3,4-bis(2-oxapropylene)tetrahydro-3a,6a-diphenylimidazo[4,5-d]imidazole-2,5(1H,3H)-dione (121619-22-5) → 1,3,4,6-Tetrakis(acetoxymethyl)tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione (154230-91-8)

Guidance literature:

With toluene-4-sulfonic acid; at 110 ℃; for 3h;

DOI:10.1002/recl.19931121207

Reference yield:

3a,6a-diphenylglycoluril (5157-15-3) → 1,3,4,6-Tetrakis(acetoxymethyl)tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione (154230-91-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent

DOI:10.1021/jo00010a001

Reference yield:

benzil (134-81-6) → 1,3,4,6-Tetrakis(acetoxymethyl)tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione (154230-91-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 89 percent / acid

2: 75 percent

With acid;

DOI:10.1021/jo00010a001

upstream raw materials:

acetic anhydride

1,6:3,4-bis(2-oxapropylene)tetrahydro-3a,6a-diphenylimidazo[4,5-d]imidazole-2,5(1H,3H)-dione

3a,6a-diphenylglycoluril

benzil

Downstream raw materials:

1,3,4,6-Tetrakis(chloromethyl)tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione

5,7,12,13b,13c,14-Hexahydro-1,4,8,11-tetramethoxy-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz<5,6>azuleno<2,1,8-ija>benzazulene-6,13-dione

5,7,12,13b,13c,14-hexahydro-1,4-dimethoxy-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz<5,6>azuleno<2,1,8-ija>benzazulene-6,13-dione

17b,17c-Dihydro-1,6,10,15-tetrahydroxy-17b,17c-diphenyl-7H,8H,9H,16H,17H,18H-7a,8a,16a,17a-tetraazapentaleno<1'',6'':5,6,7; 3'',4'',:5',6',7'>dicycloocta<1,2,3-de:1',2',3''-d'e'>dinaphthalene-8,17-dione

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