Technology Process of C24H27FN8O3
There total 7 articles about C24H27FN8O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 0 - 23 ℃;
for 15h;
DOI:10.1021/jm301626p
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 70 °C
2: sodium hydrogencarbonate / N,N-dimethyl-formamide / 30 h / 60 - 70 °C
3: triethylamine / dichloromethane / 15 h / 0 - 23 °C
With
sodium hydrogencarbonate; potassium carbonate; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301626p
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / methanol / 13 h / 23 °C / Inert atmosphere
2: sodium hydroxide; potassium permanganate / tetrahydrofuran / 72 h / 0 - 23 °C
3: sodium hydrogencarbonate / N,N-dimethyl-formamide / 30 h / 60 - 70 °C
4: triethylamine / dichloromethane / 15 h / 0 - 23 °C
With
potassium permanganate; sodium hydrogencarbonate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301626p