C₅₄H₈₄O₉Si₂

Base Information

Chemical Name:C₅₄H₈₄O₉Si₂
CAS No.:221388-73-4
Molecular Formula:C₅₄H₈₄O₉Si₂
Molecular Weight:933.427
Hs Code.:

C<sub>54</sub>H<sub>84</sub>O<sub>9</sub>Si<sub>2</sub>

Synonyms:C₅₄H₈₄O₉Si₂

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Chemical Property of C₅₄H₈₄O₉Si₂

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Technology Process of C₅₄H₈₄O₉Si₂

There total 8 articles about C₅₄H₈₄O₉Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 221388-70-1
C₅₄H₈₂O₉Si₂

: 221388-73-4
C₅₄H₈₄O₉Si₂

Guidance literature:: With hydrido(triphenylphosphine)copper(I) hexamer; In benzene; at 25 ℃; for 72h;
DOI:10.1002/(SICI)1521-3765(19990201)5:2<646::AID-CHEM646>3.0.CO;2-E

Reference yield:

: 221380-85-4
C₄₆H₆₆O₈Si

: 221388-73-4
C₅₄H₈₄O₉Si₂

Guidance literature:: Multi-step reaction with 7 steps

1: 90 percent / KHMDS / tetrahydrofuran; toluene / 2 h / -78 °C

2: 90 percent / LiCl / / tetrahydrofuran / 2 h / 70 °C

3: O₂, tetraphenylporphyrin / CCl₄ / 0.25 h / 25 °C / Irradiation

4: 58 percent / Al(Hg), H₂O, Et₃N / tetrahydrofuran / 2 h / 25 °C

5: 91 percent / imidazole / CH₂Cl₂ / 1 h / 25 °C

6: 82 percent / 4 Angstroem molecular sieves, N-methylmorpholine oxide, TPAP / CH₂Cl₂ / 3 h / 25 °C

7: 70 percent / 3PCuH>6 / benzene / 72 h / 25 °C

With 1H-imidazole; aluminum amalgam; tetrapropylammonium perruthennate; hydrido(triphenylphosphine)copper(I) hexamer; 4 A molecular sieve; water; oxygen; 5,15,10,20-tetraphenylporphyrin; potassium hexamethylsilazane; 4-methylmorpholine N-oxide; triethylamine; lithium chloride; ; In tetrahydrofuran; tetrachloromethane; dichloromethane; toluene; benzene;
DOI:10.1002/(SICI)1521-3765(19990201)5:2<646::AID-CHEM646>3.0.CO;2-E

Reference yield:

: 221388-51-8
C₅₈H₇₅O₁₁PSi

: 221388-73-4
C₅₄H₈₄O₉Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: 90 percent / LiCl / / tetrahydrofuran / 2 h / 70 °C

2: O₂, tetraphenylporphyrin / CCl₄ / 0.25 h / 25 °C / Irradiation

3: 58 percent / Al(Hg), H₂O, Et₃N / tetrahydrofuran / 2 h / 25 °C

4: 91 percent / imidazole / CH₂Cl₂ / 1 h / 25 °C

5: 82 percent / 4 Angstroem molecular sieves, N-methylmorpholine oxide, TPAP / CH₂Cl₂ / 3 h / 25 °C

6: 70 percent / 3PCuH>6 / benzene / 72 h / 25 °C

With 1H-imidazole; aluminum amalgam; tetrapropylammonium perruthennate; hydrido(triphenylphosphine)copper(I) hexamer; 4 A molecular sieve; water; oxygen; 5,15,10,20-tetraphenylporphyrin; 4-methylmorpholine N-oxide; triethylamine; lithium chloride; ; In tetrahydrofuran; tetrachloromethane; dichloromethane; benzene;
DOI:10.1002/(SICI)1521-3765(19990201)5:2<646::AID-CHEM646>3.0.CO;2-E