2-[4-(2,2-bis-ethoxycarbonyl-hexyl)-2,5-dimethylbenzyl]-2-butylmalonic acid diethyl ester

Base Information

Chemical Name:2-[4-(2,2-bis-ethoxycarbonyl-hexyl)-2,5-dimethylbenzyl]-2-butylmalonic acid diethyl ester
CAS No.:1268257-83-5
Molecular Formula:C₃₂H₅₀O₈
Molecular Weight:562.744
Hs Code.:

Synonyms:2-[4-(2,2-bis-ethoxycarbonyl-hexyl)-2,5-dimethylbenzyl]-2-butylmalonic acid diethyl ester

Suppliers and Price of 2-[4-(2,2-bis-ethoxycarbonyl-hexyl)-2,5-dimethylbenzyl]-2-butylmalonic acid diethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-[4-(2,2-bis-ethoxycarbonyl-hexyl)-2,5-dimethylbenzyl]-2-butylmalonic acid diethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-[4-(2,2-bis-ethoxycarbonyl-hexyl)-2,5-dimethylbenzyl]-2-butylmalonic acid diethyl ester

There total 2 articles about 2-[4-(2,2-bis-ethoxycarbonyl-hexyl)-2,5-dimethylbenzyl]-2-butylmalonic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 35168-62-8
2,5-dibromomethyl-p-xylene

: 133-08-4
diethyl butylmalonate

: 1268257-83-5
2-[4-(2,2-bis-ethoxycarbonyl-hexyl)-2,5-dimethylbenzyl]-2-butylmalonic acid diethyl ester

Guidance literature:: diethyl butylmalonate; With sodium ethanolate; In ethanol; at 20 ℃; for 0.5h; Inert atmosphere;

2,5-dibromomethyl-p-xylene; In ethanol; for 3h; Reflux; Inert atmosphere;
DOI:10.1016/j.ica.2010.10.002

Reference yield:

: 105-53-3
diethyl malonate

: 1268257-83-5
2-[4-(2,2-bis-ethoxycarbonyl-hexyl)-2,5-dimethylbenzyl]-2-butylmalonic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium ethanolate / ethanol / 0.5 h / 20 °C / Inert atmosphere

1.2: 3 h / Reflux; Inert atmosphere

2.1: sodium ethanolate / ethanol / 0.5 h / 20 °C / Inert atmosphere

2.2: 3 h / Reflux; Inert atmosphere

With sodium ethanolate; In ethanol;
DOI:10.1016/j.ica.2010.10.002

Reference yield: 68.0%

: 1268257-83-5
2-[4-(2,2-bis-ethoxycarbonyl-hexyl)-2,5-dimethylbenzyl]-2-butylmalonic acid diethyl ester

: 1268257-84-6
2,2'-(2,5-dimethyl-1,4-phenylene)bis(methylene)bis(2-butylmalonic acid)

Guidance literature:: 2-[4-(2,2-bis-ethoxycarbonyl-hexyl)-2,5-dimethylbenzyl]-2-butylmalonic acid diethyl ester; With potassium hydroxide; In ethanol; water; Inert atmosphere;

With hydrogenchloride; In ethanol; water; pH=3; Inert atmosphere;
DOI:10.1016/j.ica.2010.10.002