(1S,2S,5R)-(+)-neomenthyl neryl selenide

Base Information

Chemical Name:(1S,2S,5R)-(+)-neomenthyl neryl selenide
CAS No.:1462351-67-2
Molecular Formula:C₂₀H₃₆Se
Molecular Weight:355.466
Hs Code.:

Synonyms:(1S,2S,5R)-(+)-neomenthyl neryl selenide

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Chemical Property of (1S,2S,5R)-(+)-neomenthyl neryl selenide

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Technology Process of (1S,2S,5R)-(+)-neomenthyl neryl selenide

There total 4 articles about (1S,2S,5R)-(+)-neomenthyl neryl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 20536-36-1
neryl chloride

: 1462351-55-8
(1S,2S,5R)-(+)-neomenthyl selenol

: 1462351-67-2
(1S,2S,5R)-(+)-neomenthyl neryl selenide

Guidance literature:: (1S,2S,5R)-(+)-neomenthyl selenol; With n-butyllithium; In tetrahydrofuran; at -25 ℃; for 0.5h; Inert atmosphere;

neryl chloride; In tetrahydrofuran; at 0 - 50 ℃; for 1h;
DOI:10.1016/j.tetasy.2013.07.018

Reference yield:

: 2216-51-5
(-)-menthol

: 1462351-67-2
(1S,2S,5R)-(+)-neomenthyl neryl selenide

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / 24 h / 20 °C

2.1: sodium hydroxide; selenium; hydrazine hydrate

3.1: n-butyllithium / tetrahydrofuran / 0.5 h / -25 °C / Inert atmosphere

3.2: 1 h / 0 - 50 °C

With pyridine; selenium; n-butyllithium; hydrazine hydrate; sodium hydroxide; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2013.07.018

Reference yield:

: 2230-82-2
menthyl tosylate

: 1462351-67-2
(1S,2S,5R)-(+)-neomenthyl neryl selenide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide; selenium; hydrazine hydrate

2.1: n-butyllithium / tetrahydrofuran / 0.5 h / -25 °C / Inert atmosphere

2.2: 1 h / 0 - 50 °C

With selenium; n-butyllithium; hydrazine hydrate; sodium hydroxide; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2013.07.018