tert-butyl 4-(2-methoxy-6-pentadecylbenzyl)-1,4-diazepane-1-carboxylate

Base Information

Chemical Name:tert-butyl 4-(2-methoxy-6-pentadecylbenzyl)-1,4-diazepane-1-carboxylate
CAS No.:1363400-80-9
Molecular Formula:C₃₃H₅₈N₂O₃
Molecular Weight:530.835
Hs Code.:

Synonyms:tert-butyl 4-(2-methoxy-6-pentadecylbenzyl)-1,4-diazepane-1-carboxylate

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Chemical Property of tert-butyl 4-(2-methoxy-6-pentadecylbenzyl)-1,4-diazepane-1-carboxylate

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Technology Process of tert-butyl 4-(2-methoxy-6-pentadecylbenzyl)-1,4-diazepane-1-carboxylate

There total 4 articles about tert-butyl 4-(2-methoxy-6-pentadecylbenzyl)-1,4-diazepane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.8%

: 1361955-58-9
methanesulfonic acid 2-methoxy-6-pentadecyl-benzyl ester

: 112275-50-0
tert-butyl 1,4-diazepine-1-carboxylate

: 1363400-80-9
tert-butyl 4-(2-methoxy-6-pentadecylbenzyl)-1,4-diazepane-1-carboxylate

Guidance literature:: With triethylamine; In acetonitrile; at 85 ℃;
DOI:10.2174/157018011796235167

Reference yield:

: 16611-84-0
6-Pentadecylsalicylic Acid

: 1363400-80-9
tert-butyl 4-(2-methoxy-6-pentadecylbenzyl)-1,4-diazepane-1-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile / 24 h / 90 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 18.67 h / 0 - 20 °C

3: triethylamine / dichloromethane / 3.25 h / 0 - 20 °C

4: triethylamine / acetonitrile / 85 °C

With lithium aluminium tetrahydride; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.2174/157018011796235167

Reference yield:

: 65446-29-9
2-methoxy-6-pentadecyl-benzoic acid methyl ester

: 1363400-80-9
tert-butyl 4-(2-methoxy-6-pentadecylbenzyl)-1,4-diazepane-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 18.67 h / 0 - 20 °C

2: triethylamine / dichloromethane / 3.25 h / 0 - 20 °C

3: triethylamine / acetonitrile / 85 °C

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.2174/157018011796235167