1-[(E)-3-(3,4-dimethoxyphenyl)-2-propenyloxy]-1-(3,4-methylenedioxyphenyl)-2-nitro-1-propanol

Base Information

Chemical Name:1-[(E)-3-(3,4-dimethoxyphenyl)-2-propenyloxy]-1-(3,4-methylenedioxyphenyl)-2-nitro-1-propanol
CAS No.:1017684-59-1
Molecular Formula:C₂₁H₂₃NO₈
Molecular Weight:417.416
Hs Code.:

Synonyms:1-[(E)-3-(3,4-dimethoxyphenyl)-2-propenyloxy]-1-(3,4-methylenedioxyphenyl)-2-nitro-1-propanol

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Chemical Property of 1-[(E)-3-(3,4-dimethoxyphenyl)-2-propenyloxy]-1-(3,4-methylenedioxyphenyl)-2-nitro-1-propanol

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Technology Process of 1-[(E)-3-(3,4-dimethoxyphenyl)-2-propenyloxy]-1-(3,4-methylenedioxyphenyl)-2-nitro-1-propanol

There total 4 articles about 1-[(E)-3-(3,4-dimethoxyphenyl)-2-propenyloxy]-1-(3,4-methylenedioxyphenyl)-2-nitro-1-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1017684-58-0
1-[(E)-3-(3,4-dimethoxyphenyl)-2-propenyloxy]-1-(3,4-methylenedioxyphenyl)-2-nitroethane

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1017684-59-1
1-[(E)-3-(3,4-dimethoxyphenyl)-2-propenyloxy]-1-(3,4-methylenedioxyphenyl)-2-nitro-1-propanol

Guidance literature:: With potassium fluoride; In dimethyl sulfoxide; at 20 ℃; for 3h;
DOI:10.1271/bbb.60575

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 1017684-59-1
1-[(E)-3-(3,4-dimethoxyphenyl)-2-propenyloxy]-1-(3,4-methylenedioxyphenyl)-2-nitro-1-propanol

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / sodium hydroxide / methanol; H₂O / 1 h / 10 - 15 °C

2: 74 percent / KHSO₄ / toluene / 1 h / Heating

3: 62 percent / NaH / various solvent(s); hexane; tetrahydrofuran / 2 h / -78 °C

4: 46 percent / KF / dimethylsulfoxide / 3 h / 20 °C

With potassium fluoride; sodium hydroxide; potassium hydrogensulfate; sodium hydride; In tetrahydrofuran; methanol; hexane; water; dimethyl sulfoxide; toluene;
DOI:10.1271/bbb.60575

Reference yield:

: 1485-00-3,22568-48-5
5-((E)-2-nitroethenyl)-1,3-benzodioxole

: 1017684-59-1
1-[(E)-3-(3,4-dimethoxyphenyl)-2-propenyloxy]-1-(3,4-methylenedioxyphenyl)-2-nitro-1-propanol

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / NaH / various solvent(s); hexane; tetrahydrofuran / 2 h / -78 °C

2: 46 percent / KF / dimethylsulfoxide / 3 h / 20 °C

With potassium fluoride; sodium hydride; In tetrahydrofuran; hexane; dimethyl sulfoxide;
DOI:10.1271/bbb.60575