phenyl 4-O-benzoyl-1-phenylsulfanyl-2-thio-1-deoxy-β-D-fructopyranoside

Base Information

Chemical Name:phenyl 4-O-benzoyl-1-phenylsulfanyl-2-thio-1-deoxy-β-D-fructopyranoside
CAS No.:445299-11-6
Molecular Formula:C₂₅H₂₄O₅S₂
Molecular Weight:468.595
Hs Code.:

Synonyms:phenyl 4-O-benzoyl-1-phenylsulfanyl-2-thio-1-deoxy-β-D-fructopyranoside

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Chemical Property of phenyl 4-O-benzoyl-1-phenylsulfanyl-2-thio-1-deoxy-β-D-fructopyranoside

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Technology Process of phenyl 4-O-benzoyl-1-phenylsulfanyl-2-thio-1-deoxy-β-D-fructopyranoside

There total 3 articles about phenyl 4-O-benzoyl-1-phenylsulfanyl-2-thio-1-deoxy-β-D-fructopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 98-88-4
benzoyl chloride

: 445377-31-1
phenyl 1-phenylsulfanyl-2-thio-1-deoxy-β-D-fructopyranoside

: 445299-11-6
phenyl 4-O-benzoyl-1-phenylsulfanyl-2-thio-1-deoxy-β-D-fructopyranoside

Guidance literature:: phenyl 1-phenylsulfanyl-2-thio-1-deoxy-β-D-fructopyranoside; With 4 A molecular sieve; di(n-butyl)tin oxide; In acetonitrile; for 5h; Heating;

benzoyl chloride; In acetonitrile; at 20 ℃; for 16h;
DOI:10.1016/S0040-4020(02)00233-8

Reference yield:

: 108-98-5
thiophenol

: 445299-11-6
phenyl 4-O-benzoyl-1-phenylsulfanyl-2-thio-1-deoxy-β-D-fructopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: BF₃*Et₂O / CH₂Cl₂ / 14 h / 20 °C

1.2: 51 percent / Et₃N; H₂O / methanol / 16 h / 40 °C

2.1: Bu₂SnO; 4 Angstroem molecular sieves / acetonitrile / 5 h / Heating

2.2: 70 percent / acetonitrile / 16 h / 20 °C

With 4 A molecular sieve; boron trifluoride diethyl etherate; di(n-butyl)tin oxide; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(02)00233-8

Reference yield:

: 99042-47-4
2'-chloroethyl 1,3,4,5-tetra-O-acetyl-β-D-fructopyranoside

: 445299-11-6
phenyl 4-O-benzoyl-1-phenylsulfanyl-2-thio-1-deoxy-β-D-fructopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: BF₃*Et₂O / CH₂Cl₂ / 14 h / 20 °C

1.2: 51 percent / Et₃N; H₂O / methanol / 16 h / 40 °C

2.1: Bu₂SnO; 4 Angstroem molecular sieves / acetonitrile / 5 h / Heating

2.2: 70 percent / acetonitrile / 16 h / 20 °C

With 4 A molecular sieve; boron trifluoride diethyl etherate; di(n-butyl)tin oxide; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(02)00233-8