4,4,6,6-tetrachloro-3-benzyl-3,4-dihydrospiro[1.3.2]benzoxazaphosphorine[2λ5,4λ5,6λ5][1,3,5,2,4,6]triazatriphosphorine

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Chemical Name:4,4,6,6-tetrachloro-3-benzyl-3,4-dihydrospiro[1.3.2]benzoxazaphosphorine[2λ5,4λ5,6λ5][1,3,5,2,4,6]triazatriphosphorine
CAS No.:1236129-57-9
Molecular Formula:C₁₄H₁₃Cl₄N₄OP₃
Molecular Weight:488.017
Hs Code.:

Synonyms:4,4,6,6-tetrachloro-3-benzyl-3,4-dihydrospiro[1.3.2]benzoxazaphosphorine[2λ5,4λ5,6λ5][1,3,5,2,4,6]triazatriphosphorine

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Chemical Property of 4,4,6,6-tetrachloro-3-benzyl-3,4-dihydrospiro[1.3.2]benzoxazaphosphorine[2λ5,4λ5,6λ5][1,3,5,2,4,6]triazatriphosphorine

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Technology Process of 4,4,6,6-tetrachloro-3-benzyl-3,4-dihydrospiro[1.3.2]benzoxazaphosphorine[2λ5,4λ5,6λ5][1,3,5,2,4,6]triazatriphosphorine

There total 1 articles about 4,4,6,6-tetrachloro-3-benzyl-3,4-dihydrospiro[1.3.2]benzoxazaphosphorine[2λ5,4λ5,6λ5][1,3,5,2,4,6]triazatriphosphorine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 5001-26-3
2-hydroxy-N-(benzyl)benzylamine

: 1236129-57-9
4,4,6,6-tetrachloro-3-benzyl-3,4-dihydrospiro[1.3.2]benzoxazaphosphorine[2λ5,4λ5,6λ5][1,3,5,2,4,6]triazatriphosphorine

Guidance literature:: With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; triethylamine; In tetrahydrofuran; at 20 ℃; for 8h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ic100781v