2,5,6-trichloro-3-chloromethylpyridine

Base Information

• Chemical Name: 2,5,6-trichloro-3-chloromethylpyridine
• CAS No.: 52465-59-5
• Molecular Formula: C₆H₃Cl₄N
• Molecular Weight: 230.909
• Mol file: 52465-59-5.mol

Synonyms:2,5,6-trichloro-3-chloromethylpyridine

Chemical Property of 2,5,6-trichloro-3-chloromethylpyridine

Chemical Property:

• Boiling Point: 113-115 °C(Press: 0.5 Torr)
• Density: 1.579±0.06 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

2,3,6-Trichloro-5-(chloromethyl)pyridine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,5,6-trichloro-3-chloromethylpyridine

There total 2 articles about 2,5,6-trichloro-3-chloromethylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5,6-trichloro-3-chloromethyl-5,6-dehydro-piperidon-2-one + 3-chloro-3-chloromethyl-piperidine-2,6-dione (41789-40-6) → 2,5,6-trichloro-3-chloromethylpyridine (52465-59-5)

Guidance literature:

With phosphorus pentachloride; trichlorophosphate;

Reference yield:

→ 2,5,6-trichloro-3-chloromethylpyridine (52465-59-5)

Guidance literature:

Verb. (11), POCl3;

DOI:10.1002/hlca.19760590121

Reference yield: 86.0%

Hg(NO3)2 + 5H2 O + 2,5,6-trichloro-3-chloromethylpyridine (52465-59-5) → 2,5,6-Trichloronicotinic Acid (54718-39-7)

Guidance literature:

With CuSO₄; nitric acid;

upstream raw materials:

3-chloro-3-chloromethyl-piperidine-2,6-dione

Downstream raw materials:

2,5,6-Trichloronicotinic Acid

3-chloro-2,6-diaminopyridine

2,5,6-trichloro-pyridine-3-carboxylic acid chloride