(4-Methoxy-phenyl)-{5-[2-(4-methoxy-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-3-yl}-methanone

Base Information

Chemical Name:(4-Methoxy-phenyl)-{5-[2-(4-methoxy-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-3-yl}-methanone
CAS No.:147089-08-5
Molecular Formula:C₂₆H₂₁NO₃S₂
Molecular Weight:459.59
Hs Code.:

Synonyms:(4-Methoxy-phenyl)-{5-[2-(4-methoxy-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-3-yl}-methanone

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Chemical Property of (4-Methoxy-phenyl)-{5-[2-(4-methoxy-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-3-yl}-methanone

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Technology Process of (4-Methoxy-phenyl)-{5-[2-(4-methoxy-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-3-yl}-methanone

There total 3 articles about (4-Methoxy-phenyl)-{5-[2-(4-methoxy-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-3-yl}-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 2-(p-methoxyphenyl)-1,3-benzodithiolylium tetrafluoroborate

: 91917-50-9
(4-methoxyphenyl)(1H-pyrrol-3-yl)methanone

: 147089-08-5
(4-Methoxy-phenyl)-{5-[2-(4-methoxy-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-3-yl}-methanone

Guidance literature:: With pyridine; In acetonitrile; at 60 ℃; for 13h;

Reference yield:

: 91917-45-2
(1-Benzenesulfonyl-1H-pyrrol-3-yl)-(4-methoxy-phenyl)-methanone

: 147089-08-5
(4-Methoxy-phenyl)-{5-[2-(4-methoxy-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-3-yl}-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / aq. 17percent NaOH / dioxane / 15 h / Ambient temperature

2: 73 percent / pyridine / acetonitrile / 13 h / 60 °C

With pyridine; sodium hydroxide; In 1,4-dioxane; acetonitrile;

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 147089-08-5
(4-Methoxy-phenyl)-{5-[2-(4-methoxy-phenyl)-benzo[1,3]dithiol-2-yl]-1H-pyrrol-3-yl}-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / anhydrous AlCl₃ / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 97 percent / aq. 17percent NaOH / dioxane / 15 h / Ambient temperature

3: 73 percent / pyridine / acetonitrile / 13 h / 60 °C

With pyridine; sodium hydroxide; aluminium trichloride; In 1,4-dioxane; dichloromethane; acetonitrile;