4-((S)-5-Phenoxymethyl-3-trimethylsilanyl-4,5-dihydro-furan-2-yl)-morpholine

Base Information

Chemical Name:4-((S)-5-Phenoxymethyl-3-trimethylsilanyl-4,5-dihydro-furan-2-yl)-morpholine
CAS No.:415902-43-1
Molecular Formula:C₁₈H₂₇NO₃Si
Molecular Weight:333.503
Hs Code.:

Synonyms:4-((S)-5-Phenoxymethyl-3-trimethylsilanyl-4,5-dihydro-furan-2-yl)-morpholine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-((S)-5-Phenoxymethyl-3-trimethylsilanyl-4,5-dihydro-furan-2-yl)-morpholine

Chemical Property:

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Technology Process of 4-((S)-5-Phenoxymethyl-3-trimethylsilanyl-4,5-dihydro-furan-2-yl)-morpholine

There total 3 articles about 4-((S)-5-Phenoxymethyl-3-trimethylsilanyl-4,5-dihydro-furan-2-yl)-morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64024-63-1
1-morpholino-2-trimethylsilyl acetylene

: 71031-03-3,71031-02-2
(R)-phenyl glycidyl ether

: 415902-43-1
4-((S)-5-Phenoxymethyl-3-trimethylsilanyl-4,5-dihydro-furan-2-yl)-morpholine

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1021/ja025604c

Reference yield:

: 60506-50-5
1,1,2-Trichloro-2-morpholinoethen

: 415902-43-1
4-((S)-5-Phenoxymethyl-3-trimethylsilanyl-4,5-dihydro-furan-2-yl)-morpholine

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / diethyl ether; hexane / -78 - 23 °C

1.2: 75 percent / diethyl ether; hexane / 15 h / 23 °C

2.1: boron trifluoride diethyl etherate / CH₂Cl₂ / 0.5 h / 0 °C

With n-butyllithium; boron trifluoride diethyl etherate; In diethyl ether; hexane; dichloromethane;
DOI:10.1021/ja025604c

Reference yield:

: 13306-60-0
N-(trichloroacetyl)morpholine

: 415902-43-1
4-((S)-5-Phenoxymethyl-3-trimethylsilanyl-4,5-dihydro-furan-2-yl)-morpholine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 80 percent / o-xylene / 1.5 h / 150 °C

2.1: n-butyllithium / diethyl ether; hexane / -78 - 23 °C

2.2: 75 percent / diethyl ether; hexane / 15 h / 23 °C

3.1: boron trifluoride diethyl etherate / CH₂Cl₂ / 0.5 h / 0 °C

With n-butyllithium; boron trifluoride diethyl etherate; In diethyl ether; hexane; dichloromethane; o-xylene;
DOI:10.1021/ja025604c